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The Exfoliation of Graphene in Liquids by Electrochemical, Chemical, and Sonication‐Assisted Techniques: A Nanoscale Study
Abstract
The different exfoliation routes of graphite to produce graphene by sonication in solvent, chemical oxidation and electrochemical oxidation are compared. The exfoliation process and roughening of a flat graphite substrate is directly visualized at the nanoscale by scanning probe and electron microscopy. The etching damage in graphite and the properties of the exfoliated sheets are compared by Raman spectroscopy and X‐ray diffraction analysis. The results show the trade‐off between exfoliation speed and preservation of graphene quality. A key step to achieve efficient exfoliation is to couple gas production and mechanical exfoliation on a macroscale with non‐covalent exfoliation and preservation of graphene properties on a molecular scale.
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Citations
Cites
The chemistry of graphene oxide
Dreyer, D. R., Park, S., Bielawski, C. W., & Ruoff, R. S. (2010) · Chem. Soc. Rev. · doi:10.1039/b917103g · Cited by 11,653
Cited by
Two‐Dimensional Nanostructured Materials for Gas Sensing
Liu, X., Ma, T., Pinna, N., & Zhang, J. (2017) · Advanced Functional Materials · doi:10.1002/adfm.201702168 · Cited by 851
Hou, Y., Lohe, M. R., Zhang, J., Liu, S., Zhuang, X., & Feng, X. (2016) · Energy & Environmental Science · doi:10.1039/c5ee03440j · Cited by 824
Liu, Z., Wu, Z., Yang, S., Dong, R., Feng, X., & Müllen, K. (2016) · Advanced Materials · doi:10.1002/adma.201505304 · Cited by 411
Synthesis, structure and applications of graphene-based 2D heterostructures
Solís-Fernández, P., Bissett, M., & Ago, H. (2017) · Chemical Society Reviews · doi:10.1039/c7cs00160f · Cited by 371
New‐Generation Graphene from Electrochemical Approaches: Production and Applications
Yang, S., Lohe, M. R., Müllen, K., & Feng, X. (2016) · Advanced Materials · doi:10.1002/adma.201505326 · Cited by 313
Metadata
- Authors
- Xia, Z. Y., Pezzini, S., Treossi, E., Giambastiani, G., Corticelli, F., Morandi, V., Zanelli, A., Bellani, V., & Palermo, V.
- Venue
- Advanced Functional Materials
- Publisher
- Wiley
- Published
- 2013-04-17
- Volume
- 23
- Issue
- 37
- Pages
- 4684-4693
- ISSN
- 1616-301X (ISSN-L)
- 1616-3028
- OpenAlex
- W2098638390
- Cited by
- 234
- References
- 1
- FWCI
- 8.88
- Type
- journal article
- Language
- en
- Open access
- closed
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- The paper
- Xia, Z. Y., Pezzini, S., Treossi, E., Giambastiani, G., Corticelli, F., Morandi, V., Zanelli, A., Bellani, V., & Palermo, V. (2013). The Exfoliation of Graphene in Liquids by Electrochemical, Chemical, and Sonication‐Assisted Techniques: A Nanoscale Study. Advanced Functional Materials. https://doi.org/10.1002/adfm.201203686
Data sources
Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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