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Pt@MOF‐177: Synthesis, Room‐Temperature Hydrogen Storage and Oxidation Catalysis
Abstract
The gas‐phase loading of [Zn 4 O(btb)2]8 (MOF‐177; H 3 btb=1,3,5‐benzenetribenzoic acid) with the volatile platinum precursor [Me 3 PtCp′] (Cp′=methylcyclopentadienyl) was confirmed by solid state 13 C magic angle spinning (MAS)‐NMR spectroscopy. Subsequent reduction of the inclusion compound [Me 3 PtCp′]4@MOF‐177 by hydrogen at 100 bar and 100 °C for 24 h was carried out and gave rise to the formation of platinum nanoparticles in a size regime of 2–5 nm embedded in the unchanged MOF‐177 host lattice as confirmed by transmission electron microscopy (TEM) micrographs and powder X‐ray diffraction (PXRD). The room‐temperature hydrogen adsorption of Pt@MOF‐177 has been followed in a gravimetric fashion (magnetic suspension balance) and shows almost 2.5 wt % in the first cycle, but is decreased down to 0.5 wt % in consecutive cycles. The catalytic activity of Pt@MOF‐177 towards the solvent‐ and base‐free room temperature oxidation of alcohols in air has been tested and shows Pt@MOF‐177 to be an efficient catalyst in the oxidation of alcohols.
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Citations
Cites
Millward, A. R., & Yaghi, O. M. (2005) · Journal of the American Chemical Society · doi:10.1021/ja0570032 · Cited by 2,876
Materials for hydrogen storage
Züttel, A. (2003) · Materials Today · doi:10.1016/s1369-7021(03)00922-2 · Cited by 2,216
Cited by
Multifunctional metal–organic framework catalysts: synergistic catalysis and tandem reactions
Huang, Y.-B., Liang, J., Wang, X.-S., & Cao, R. (2017) · Chemical Society Reviews · doi:10.1039/c6cs00250a · Cited by 1,908
Metadata
- Authors
- Proch, S., Herrmannsdörfer, J., Kempe, R., Kern, C., Jess, A., Seyfarth, L., & Senker, J.
- Venue
- Chemistry – A European Journal
- Publisher
- Wiley
- Published
- 2008-09-15
- Volume
- 14
- Issue
- 27
- Pages
- 8204-8212
- ISSN
- 0947-6539 (ISSN-L)
- 1521-3765
- OpenAlex
- W2140519903
- Cited by
- 311
- References
- 2
- FWCI
- 12.01
- Type
- journal article
- Language
- en
- Open access
- closed
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- Proch, S., Herrmannsdörfer, J., Kempe, R., Kern, C., Jess, A., Seyfarth, L., & Senker, J. (2008). Pt@MOF‐177: Synthesis, Room‐Temperature Hydrogen Storage and Oxidation Catalysis. Chemistry – A European Journal. https://doi.org/10.1002/chem.200801043
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