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Elucidation of Lignin Structure by Quantitative 2D NMR

Sette, Marco, Wechselberger, Rainer, Crestini, Claudia·2011·Chemistry – A European Journal

Abstract

Quick quantitative HSQC (QQ‐HSQC) was applied to quantitative evaluation of different inter‐unit linkages in an array of milled softwood and hardwood and technical lignins by using the guaiacyl C2 and syringyl C2–C6 signals as internal standards. The results were found to be highly reproducible and comparable with earlier literature reports. The advantage of QQ‐HSQC NMR analysis of lignin is contemporary detection and quantification of lignin inter‐unit linkages with a direct, non‐destructive method requiring short acquisition times.

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Metadata

Authors
Sette, M., Wechselberger, R., & Crestini, C.
Venue
Chemistry – A European Journal
Publisher
Wiley
Published
2011-06-30
Volume
17
Issue
34
Pages
9529-9535
ISSN
  • 0947-6539 (ISSN-L)
  • 1521-3765
OpenAlex
W2161469143
Cited by
336
References
0
FWCI
7.11
Type
journal article
Language
en
Open access
closed

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Sette, M., Wechselberger, R., & Crestini, C. (2011). Elucidation of Lignin Structure by Quantitative 2D NMR. Chemistry – A European Journal. https://doi.org/10.1002/chem.201003045

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