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Direct Synthesis of 1,6‐Hexanediol from HMF over a Heterogeneous Pd/ZrP Catalyst using Formic Acid as Hydrogen Source
Abstract
A new approach is developed for hydrogenolytic ring opening of biobased 5‐hydroxymethylfurfural (HMF), dehydration product of hexoses, towards 1,6‐hexanediol (HDO) under atmospheric pressure. The highest yield of HDO, 43 %, is achieved over reusable Pd/zirconium phosphate (ZrP) catalyst at 413 K in the presence of formic acid as hydrogen source. In comparison with various Brønsted and/or Lewis acidic supports, the specific Brønsted acidity on ZrP support effectively accelerated the cleavage of CO bond in a furan ring.
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Cites
Chemical Routes for the Transformation of Biomass into Chemicals
Corma, A., Iborra, S., & Velty, A. (2007) · Chemical Reviews · doi:10.1021/cr050989d · Cited by 5,970
Efficient Dehydrogenation of Formic Acid Using an Iron Catalyst
Boddien, A., Mellmann, D., Gärtner, F., Jackstell, R., Junge, H., Dyson, P. J., Laurenczy, G., Ludwig, R., & Beller, M. (2011) · Science · doi:10.1126/science.1206613 · Cited by 832
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Hu, L., Lin, L., Wu, Z., Zhou, S., & Liu, S. (2017) · Renewable and Sustainable Energy Reviews · doi:10.1016/j.rser.2017.02.042 · Cited by 445
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Zhang, Q., Song, M., Xu, Y., Wang, W., Wang, Z., & Zhang, L. (2021) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2021.101430 · Cited by 433
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Nie, R., Tao, Y., Nie, Y., Lu, T., Wang, J., Zhang, Y., Lu, X., & Xu, C. C. (2021) · ACS Catalysis · doi:10.1021/acscatal.0c04939 · Cited by 341
Metadata
- Authors
- Tuteja, J., Choudhary, H., Nishimura, S., & Ebitani, K.
- Venue
- ChemSusChem
- Publisher
- Wiley
- Published
- 2013-11-20
- Volume
- 7
- Issue
- 1
- Pages
- 96-100
- ISSN
- 1864-5631 (ISSN-L)
- 1864-564X
- OpenAlex
- W2016481574
- Cited by
- 232
- References
- 2
- FWCI
- 9.21
- Type
- journal article
- Language
- en
- Open access
- closed
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