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Hydrolysis of aluminium alkoxides and bayerite conversion
Abstract
A study of hydrolysis of aluminium alkoxides as a function of water temperature, and structural transformation of the resultant hydroxides was conducted. Hot water hydrolysis of aluminium alkoxides produces boehmite, whereas cold water hydrolysis results in formation of amorphous monohydroxide. This amorphous phase contains OR groups whose removal by water during aging causes the material to convert to bayerite or boehmite. Bayerite conversion takes place below 80 °C by a dissolution‐recrystallisation process in which the gradual liberation of OR groups by water appears to play an important role. Boehmite conversion takes place above 80 °C where vigorous liberation of OR groups occurs and the slow stoichiometric bayerite conversion diminishes. Neither conversion takes place in pure alcohol.
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Citations
Cites
Crystallization processes in aluminium hydroxide gels
Bye, G. C., & Robinson, J. G. (1964) · Kolloid-Zeitschrift & Zeitschrift für Polymere · doi:10.1007/bf01499454 · Cited by 92
Electron microscope studies on the aging of amorphous colloidal aluminium hydroxide
Santos, P. S., Vallejo-Freire, A., & Santos, H. L. S. (1953) · Colloid & Polymer Science · doi:10.1007/bf01513437 · Cited by 53
Cited by
Aluminum Hydroxides and Oxyhydroxides
Hsu, P. H. (1989) · SSSA Book Series · doi:10.2136/sssabookser1.2ed.c7 · Cited by 231
An overview on alumina-silica-based aerogels
Almeida, C. M. R., Ghica, M. E., & Durães, L. (2020) · Advances in Colloid and Interface Science · doi:10.1016/j.cis.2020.102189 · Cited by 132
Metadata
- Authors
- Yoldas, B. E.
- Venue
- Journal of Applied Chemistry and Biotechnology
- Publisher
- Wiley
- Published
- 1973-11
- Volume
- 23
- Issue
- 11
- Pages
- 803-809
- ISSN
- 0375-9210 (ISSN-L)
- 1935-0554
- OpenAlex
- W2026833109
- Cited by
- 301
- References
- 2
- FWCI
- 2.13
- Type
- journal article
- Language
- en
- Open access
- closed
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