The DOI matches its Crossref record; 2 of the 2 references it cites were found in a registry or an index.
On the Interpretation of X‐Ray Diffraction Powder Patterns in Terms of the Nanostructure of Cellulose I Fibres
Abstract
Summary: The average lateral dimensions of cellulose microfibrils in paper sheets can be determined from the width of X‐ray Bragg peaks at half the maximum height. The method assumes it is the finite size of the crystallite which is the main contributor to peak broadening in the directions orthogonal to the long axis of the crystallite. This assumption is examined in the context of samples from different botanical sources, of varying crystallinity and cellulose content and the various instrumental sources of broadening X‐ray powder patterns. Excellent fits to the data from paper samples can be obtained by using five Voigt functions to the powder diffraction patterns, for the 101, $10\bar 1$, 021, 002 and 040 reflections. Of these reflections, the 020 is the clearest, and the best able to determine the lateral dimension of the crystallite. Results indicate that the size of microfibrils is dependent on the botanical source of the fibres. magnified image
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Cites
Sugiyama, J., Vuong, R., & Chanzy, H. (1991) · Macromolecules · doi:10.1021/ma00014a033 · Cited by 791
Combined infrared and electron diffraction study of the polymorphism of native celluloses
Sugiyama, J., Persson, J., & Chanzy, H. (1991) · Macromolecules · doi:10.1021/ma00009a050 · Cited by 541
Cited by
Park, S., Baker, J. O., Himmel, M. E., Parilla, P. A., & Johnson, D. K. (2010) · Biotechnology for Biofuels · doi:10.1186/1754-6834-3-10 · Cited by 3,395
Comparison and assessment of methods for cellulose crystallinity determination
Salem, K. S., Kasera, N. K., Rahman, M. A., Jameel, H., Habibi, Y., Eichhorn, S. J., French, A. D., Pal, L., & Lucia, L. A. (2023) · Chemical Society Reviews · doi:10.1039/d2cs00569g · Cited by 600
Cheng, G., Varanasi, P., Li, C., Liu, H., Melnichenko, Y. B., Simmons, B. A., Kent, M. S., & Singh, S. (2011) · Biomacromolecules · doi:10.1021/bm101240z · Cited by 437
Dalle Vacche, S., Karunakaran, V., Patrucco, A., Zoccola, M., Douard, L., Ronchetti, S., Gallo, M., Schreier, A., Leterrier, Y., Bras, J., et al. (2021) · Molecules · doi:10.3390/molecules26164723 · Cited by 32
Metadata
- Authors
- Garvey, C. J., Parker, I. H., & Simon, G. P.
- Venue
- Macromolecular Chemistry and Physics
- Publisher
- Wiley
- Published
- 2005-07-29
- Volume
- 206
- Issue
- 15
- Pages
- 1568-1575
- ISSN
- 1022-1352 (ISSN-L)
- 1521-3935
- OpenAlex
- W2102648763
- Cited by
- 308
- References
- 2
- FWCI
- 0.49
- Type
- journal article
- Language
- en
- Open access
- closed
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- Garvey, C. J., Parker, I. H., & Simon, G. P. (2005). On the Interpretation of X‐Ray Diffraction Powder Patterns in Terms of the Nanostructure of Cellulose I Fibres. Macromolecular Chemistry and Physics. https://doi.org/10.1002/macp.200500008
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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