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Use of eugenol and rosin as feedstocks for biobased epoxy resins and study of curing and performance properties
Abstract
In this study, an epoxy based on eugenol and an anhydride curing agent based on rosin were prepared. Curing of the eugenol epoxy with a commercial anhydride curing agent and with the rosin‐derived anhydride curing agent was studied. For comparison, a commercial bisphenol A type epoxy, DER353 , was also selected in the curing study. The syntheses of the eugenol epoxy and rosin anhydride were investigated and the chemical structures of the products and intermediates were characterized using 1 H NMR and Fourier transform infrared spectroscopies. Non‐isothermal curing of the eugenol epoxy with hexahydrophthalic anhydride and the rosin‐derived maleopimaric acid was studied using differential scanning calorimetry. Thermomechanical properties and thermal stability of the cured epoxy resins were evaluated using dynamic mechanical analysis and thermogravimetric analysis, respectively. Addition of 2‐ethyl‐4‐methylimidazole as catalyst greatly decreased the curing temperature and promoted the completion of cure reactions. The results suggest that the eugenol epoxy and the bisphenol A type epoxy have similar reactivity, dynamic mechanical properties and thermal stability. © 2013 Society of Chemical Industry
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Feng, Y., Mu, J., Chen, S., Huang, Z., & Yu, Z. (2012) · BioResources · doi:10.15376/biores.7.4.4600-4613 · Cited by 40
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Recent advances in bio‐based epoxy resins and bio‐based epoxy curing agents
Baroncini, E. A., Kumar Yadav, S., Palmese, G. R., & Stanzione, J. F. (2016) · Journal of Applied Polymer Science · doi:10.1002/app.44103 · Cited by 451
Naturally occurring phenolic sources: monomers and polymers
Lochab, B., Shukla, S., & Varma, I. K. (2014) · RSC Adv. · doi:10.1039/c4ra00181h · Cited by 293
Metadata
- Authors
- Qin, J., Liu, H., Zhang, P., Wolcott, M., & Zhang, J.
- Venue
- Polymer International
- Publisher
- Wiley
- Published
- 2013-08-14
- Volume
- 63
- Issue
- 4
- Pages
- 760-765
- ISSN
- 0959-8103 (ISSN-L)
- 1097-0126
- OpenAlex
- W1879190489
- Cited by
- 163
- References
- 1
- FWCI
- 14.61
- Type
- journal article
- Language
- en
- Open access
- closed
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- Qin, J., Liu, H., Zhang, P., Wolcott, M., & Zhang, J. (2014). Use of eugenol and rosin as feedstocks for biobased epoxy resins and study of curing and performance properties. Polymer International. https://doi.org/10.1002/pi.4588
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