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Speciation of metals and metalloids in sediments with LTGC/ICP-MS
Abstract
Low temperature GC on-line coupled with an ICP/MS has been used as analytical device to detect organometallic and -metalloid compounds from various sediments of rivers and harbours in West Germany. The different species have been volatilized by derivatization with NaBH(4) and cryofocussed in a trap. Different alkylated species of As, Sn and Sb have been identified, while only methylated compounds of the elements Ge, Se, Te, Hg and Bi could be detected.
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Concentrations of up to 9 nM DMSe and 11 nM DMDSe have been measured in river sediments, while in river water up to 37 pM DMSe has been quantified.
“Concentrations of up to 9 nM DMSe and 11 nM DMDSe have been measured in river sediments [254], while in river water up to 37 pM DMSe has been quantified [255].”
From Selenium Cycling Across Soil-Plant-Atmosphere Interfaces: A Critical Review (2015) · cites this paper as [254]
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Selenium Cycling Across Soil-Plant-Atmosphere Interfaces: A Critical Review
Winkel, L., Vriens, B., Jones, G., Schneider, L., Pilon-Smits, E., & Bañuelos, G. (2015) · Nutrients · doi:10.3390/nu7064199 · Cited by 476
“Concentrations of up to 9 nM DMSe and 11 nM DMDSe have been measured in river sediments [254], while in river water up to 37 pM DMSe has been quantified [255].”
Metadata
- Authors
- Krupp, E. M., Gr�mping, R., Furchtbar, U. R. R., & Hirner, A. V.
- Affiliations
- University of Duisburg-Essen (DE)
- Venue
- Analytical and Bioanalytical Chemistry
- Published
- 1996-03-01
- Volume
- 354
- Issue
- 5-6
- Pages
- 546-549
- ISSN
- 1618-2642 (ISSN-L)
- 1618-2650
- OpenAlex
- W1999027961
- Cited by
- 67
- References
- 0
- Citations by year
- 2026: 2 · 2024: 1 · 2023: 1 · 2021: 1 · 2020: 4 · 2017: 1 · 2016: 1 · 2015: 3
- FWCI
- 7.31
- Type
- journal article
- Language
- en
- Open access
- closed
- Licence
- www.springer.com/tdm (tdm)
- Locations
- Analytical and Bioanalytical Chemistry (publishedVersion)
- PubMed (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical Chemistry and Chromatography
- Physical Sciences › Environmental Science › Water Science and Technology › Environmental and Analytical Chemistry Studies
- Keywords
- metal speciation, metalloids, river sediments, harbour sediments, organometallic compounds, inductively coupled plasma mass spectrometry, cryofocusing
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