Cited by 329Hydrogels: synthesis, properties, applicationsPolysaccharides Composition and ApplicationsPolymer-Based Agricultural Enhancements

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Synthesis and swelling behavior of xanthan-based hydrogels

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Bueno, Vania Blasques, Bentini, Ricardo, Catalani, Luiz Henrique, Petri, Denise Freitas Siqueira·2013·Carbohydrate Polymers

DOI 10.1016/j.carbpol.2012.10.062

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Abstract

In this work xanthan chains were crosslinked by esterification reaction at 165 °C either in the absence or in the presence of citric acid. Higher crosslinking density was obtained using citric acid, as evidenced by its lower swelling degree. Tensiometry, a very precise and sensitive technique, was applied to study swelling rates and diffusion mechanisms of water, which was initially quasi-Fickian, controlled by wicking properties, changing to Fickian or Anomalous, depending on hydrogel composition. Hydrogels swelling degree increased at high pH values, due to electrostatic repulsion and ester linkages rupture. Equilibrium swelling degree was affected by salts, depending on gel composition and kind of salt. Effects could be explained by interaction between ions and polymeric chains, EPA/EPD ability of water or osmotic gradient.

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Authors: Bueno, V. B., Bentini, R., Catalani, L. H., & Petri, D. F. S.
Affiliations: Universidade de São Paulo (BR)
ORCID: Bueno, Vania Blasques
Catalani, Luiz Henrique
Petri, Denise Freitas Siqueira
Venue: Carbohydrate Polymers
Publisher: Elsevier BV
Published: 2013-02
Volume: 92
Issue: 2
Pages: 1091-1099
ISSN: 0144-8617 (ISSN-L)
DOI: 10.1016/j.carbpol.2012.10.062
OpenAlex: W2029308143
Cited by: 329
References: 56
Citations by year: 2026: 22 · 2025: 28 · 2024: 32 · 2023: 32 · 2022: 31 · 2021: 23 · 2020: 29 · 2019: 30 · 2018: 29 · 2017: 21 · 2016: 21 · 2015: 17 · 2014: 9 · 2013: 5
FWCI: 4.58
Type: journal article
Language: en
Open access: bronze
doi.org
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
www.elsevier.com/open-access/userlicense/1.0/ (vor, 439 d)
Locations: Carbohydrate Polymers (publishedVersion)
PubMed (publishedVersion)
Funders: Brazilian Agency FAPESP
Topics: Physical Sciences › Materials Science › Biomaterials › Hydrogels: synthesis, properties, applications
Life Sciences › Agricultural and Biological Sciences › Food Science › Polysaccharides Composition and Applications
Life Sciences › Agricultural and Biological Sciences › Agronomy and Crop Science › Polymer-Based Agricultural Enhancements
Keywords: xanthan gum, hydrogels, swelling behavior, citric acid, crosslink density, water diffusion, wicking, anomalous diffusion, pH effect, salt effects, ion-polymer interactions, osmotic gradient, swelling ratio
MeSH terms: Diffusion, Hydrogen-Ion Concentration, Polysaccharides, Bacterial, Water, Citric Acid, Hydrogels, Chemistry Techniques, Synthetic

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Synthesis and swelling behavior of xanthan-based hydrogels

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