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Cited by 95Advanced Cellulose Research StudiesBiofuel production and bioconversionPolysaccharides Composition and Applications

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Carboxymethyl cellulose production from sugarcane bagasse with steam explosion pulping: Experimental, modeling, and optimization

Golbaghi, Loghman, Khamforoush, Mehrdad, Hatami, Tahmasb·2017·Carbohydrate Polymers
DOI 10.1016/j.carbpol.2017.06.123
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Abstract

The sugarcane bagasse was used for producing carboxymethyl cellulose (CMC) and obtaining high-molecular-mass hemicellulose as co-product. To this end, the steam explosion process was employed. It was found that the optimum operating conditions are the temperature of 187.15°C, NaOH/bagasse ratio of 39% (w/w), and retention time (RT) of 10min. Next, the obtained cellulose in the optimized condition was extracted and purified, and it was subsequently converted to CMC according to Williamson etherification technique. This paper also employed response surface methodology (RSM) to model effective factors against a degree of substitution (DS). Based on it, the optimum values of independent variables are the NaOH concentration of 28.4%, MCA mass of 1.14gram, temperature of 57.85°C, and reaction time of 4.01h which the CMC had the DS of 1.085, the yield of 181.302%, purity of 71.6%, and crystallinity of 30.1% with low viscosity. Samples comparatively studied by FT-IR, TGA and XRD.

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Research works printed but not linked: 36

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Metadata

Authors
Golbaghi, L., Khamforoush, M., & Hatami, T.
Affiliations
University of Kurdistan (IR)
Corresponding author
Khamforoush, Mehrdad
ORCID
Venue
Carbohydrate Polymers
Publisher
Elsevier BV
Published
2017-10
Volume
174
Pages
780-788
ISSN
0144-8617 (ISSN-L)
DOI
10.1016/j.carbpol.2017.06.123
OpenAlex
W2731887939
Cited by
95
References
0
Citations by year
2026: 12 · 2025: 10 · 2024: 11 · 2023: 15 · 2022: 14 · 2021: 11 · 2020: 11 · 2019: 7 · 2018: 4
FWCI
2.17
Type
journal article
Language
en
Open access
closed
Licence
www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations
  • Carbohydrate Polymers (publishedVersion)
  • PubMed (publishedVersion)
Funders
University of Kurdistan
Topics
  • Physical Sciences › Materials Science › Biomaterials › Advanced Cellulose Research Studies
  • Physical Sciences › Engineering › Biomedical Engineering › Biofuel production and bioconversion
  • Life Sciences › Agricultural and Biological Sciences › Food Science › Polysaccharides Composition and Applications
Keywords
carboxymethyl cellulose, sugarcane bagasse, hemicellulose, Williamson ether synthesis, degree of substitution, NaOH pretreatment, cellulose extraction, process optimization, crystallinity

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