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Quantitative determination of phases in the alkaline activation of fly ash. Part II: Degree of reaction
Abstract
A working procedure was developed for determining the degree of reaction of fly ash subjected to alkali activation (with 8 M NaOH) at mild temperatures. Since the reaction products dissolve in HCl, the residue left after this acid attack contains only the fraction of the original ash that failed to react with the basic solution. This residue was analysed with Rietveld XRPD quantification and NMR and the findings were compared to the results of the analyses run on the activated ash to obtain a very precise quantification of all of the (crystalline, vitreous and amorphous) phases present in the systems studied.
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Cited by
Geopolymer technology: The current state of the art
Duxson, P., Fernández-Jiménez, A., Provis, J. L., Lukey, G. C., Palomo, A., & van Deventer, J. S. J. (2007) · Journal of Materials Science · doi:10.1007/s10853-006-0637-z · Cited by 4,742
Self-citationAn XRD study of the effect of the SiO2/Na2O ratio on the alkali activation of fly ash
Criado, M., Fernández-Jiménez, A., de la Torre, A. G., Aranda, M. A. G., & Palomo, A. (2007) · Cement and Concrete Research · doi:10.1016/j.cemconres.2007.01.013 · Cited by 503
Self-citationIn Situ ATR-FTIR Study of the Early Stages of Fly Ash Geopolymer Gel Formation
Rees, C. A., Provis, J. L., Lukey, G. C., & van Deventer, J. S. J. (2007) · Langmuir · doi:10.1021/la701185g · Cited by 411
Effect of Alumina Release Rate on the Mechanism of Geopolymer Gel Formation
Hajimohammadi, A., Provis, J. L., & van Deventer, J. S. J. (2010) · Chemistry of Materials · doi:10.1021/cm101151n · Cited by 314
Waste glass as partial mineral precursor in alkali-activated slag/fly ash system
Zhang, S., Keulen, A., Arbi, K., & Ye, G. (2017) · Cement and Concrete Research · doi:10.1016/j.cemconres.2017.08.012 · Cited by 283
Metadata
- Authors
- Fernández-Jiménez, A., de la Torre, A. G., Palomo, A., López-Olmo, G., Alonso, M. M., & Aranda, M. A. G.
- Venue
- Fuel
- Publisher
- Elsevier BV
- Published
- 2006-10
- Volume
- 85
- Issue
- 14-15
- Pages
- 1960-1969
- ISSN
- 0016-2361 (ISSN-L)
- OpenAlex
- W2101303790
- Cited by
- 221
- References
- 0
- FWCI
- 24.64
- Type
- journal article
- Language
- en
- Open access
- closed
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- The paper
- Fernández-Jiménez, A., de la Torre, A. G., Palomo, A., López-Olmo, G., Alonso, M. M., & Aranda, M. A. G. (2006). Quantitative determination of phases in the alkaline activation of fly ash. Part II: Degree of reaction. Fuel. https://doi.org/10.1016/j.fuel.2006.04.006
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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