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Synthesis and characterization of porous tree gum grafted copolymer derived from Prunus cerasifera gum polysaccharide
Abstract
Porous grafted copolymer with excellent thermal stability and swelling capacity was synthesized from water soluble Prunus cerasifera gum polysaccharide (PG) and acrylamide (AM). The monosaccharide compositions and the structure of Prunus cerasifera tree gum were detected by a high-performance anion exchange chromatography (HPAEC) system and 1 H NMR and 13 C NMR, and the obtained PG-AM copolymer was characterized by Fourier transform infrared (FT-IR), scanning electron microscope (SEM), thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC), respectively. The results indicated that the water soluble polysaccharides obtained from Prunus cerasifera tree gum were mainly composed of l-arabinose (39.78%) and d-galactose (40.59%) with minor amount of xylose, mannose and uronic acids. The maximum percent and the grafting efficiency of grafting acrylamide (AM) onto PG to form PG-AM were obtained by copolymerization between polysaccharide and 3 times (weight) acrylamide with 3 mmol/L potassium persulfate initiator at 50 °C for 1 h. In addition, lots of isolated and conjoint pores were observed in the prepared PG-AM materials, with a diameters distribution between 2 and 10 μm. Compared with PG, the synthesized copolymer PG-AM showed an excellent performance in thermal stability and swelling capacity. The detailed structural characteristic together with excellent thermal stability and swelling properties will benefit efficient utilization of the synthesized copolymer as a precursor for preparation of large-scale environmentally friendly advanced materials with various potential applications.
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“Previously gums obtained from Prunus dulcis and Prunus cerasifera have been employed to design grafted copolymer systems (Hussain and Jaisankar 2017;Shi et al., 2019;Singh et al., 2022).”
From A novel pH-responsive hydrogel system based on Prunus armeniaca gum and acrylic acid: Preparation and evaluation as a potential candidate for controlled drug delivery. (2023) · cites this paper as Shi et al., 2019
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Cited by
Sorted by citations
Noureen, S., Noreen, S., Ghumman, S. A., Abdelrahman, E. A., Batool, F., Aslam, A., Mehdi, M., Shirinfar, B., & Ahmed, N. (2023) · European Journal of Pharmaceutical Sciences · doi:10.1016/j.ejps.2023.106555 · Cited by 28
“Previously gums obtained from Prunus dulcis and Prunus cerasifera have been employed to design grafted copolymer systems (Hussain and Jaisankar 2017; Shi et al., 2019; Singh et al., 2022).”
Method
Metadata
- Authors
- Shi, Z., Jia, C., Wang, D., Deng, J., Xu, G., Wu, C., Dong, M., & Guo, Z.
- Affiliations
- Southwest Forestry University (CN)
- Zhengzhou University (CN)
- University of Tennessee at Knoxville (US)
- Corresponding author
- Wang, Dawei
- Guo, Zhanhu
- Venue
- International Journal of Biological Macromolecules
- Publisher
- Elsevier BV
- Published
- 2019-07
- Volume
- 133
- Pages
- 964-970
- ISSN
- 0141-8130 (ISSN-L)
- OpenAlex
- W2935831871
- Cited by
- 96
- References
- 84
- Citations by year
- 2026: 5 · 2025: 5 · 2024: 7 · 2023: 7 · 2022: 6 · 2021: 3 · 2020: 18 · 2019: 45
- FWCI
- 13.89
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- International Journal of Biological Macromolecules (publishedVersion)
- PubMed (publishedVersion)
- Funders
- National Natural Science Foundation of China (31460214, 31560195, 31760195)
- Fundamental Research Funds of Yunnan Province (2018FB066)
- Guanxi Key Laboratory of Chemistry and Engineering of Forest Products (2017AD19029)
- Topics
- Life Sciences › Agricultural and Biological Sciences › Food Science › Polysaccharides Composition and Applications
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer Synthesis and Characterization
- Physical Sciences › Materials Science › Biomaterials › Hydrogels: synthesis, properties, applications
- Keywords
- acrylamide grafting, porous media, swelling power, thermal stability, monosaccharide composition, grafting efficiency, potassium persulfate initiator, polysaccharide characterization
- MeSH terms
- Prunus domestica, Monosaccharides, Polysaccharides, Temperature, Uronic Acids, Porosity, Acrylamide, Plant Gums, Polymerization, Chemistry Techniques, Synthetic
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