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Cited by 106Concrete and Cement Materials ResearchCalcium Carbonate Crystallization and InhibitionMesoporous Materials and Catalysis

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Effect of addition of silica- and amine functionalized silica-nanoparticles on the microstructure of calcium silicate hydrate (C–S–H) gel

Monasterio, Manuel, Gaitero, Juan J., Erkizia, Edurne, Guerrero Bustos, Ana M., Miccio, Luis A., Dolado, Jorge S., Cerveny, Silvina·2015·Journal of Colloid and Interface Science
DOI 10.1016/j.jcis.2015.02.066
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Abstract

In this work we study the influence of adding nano-silica (SiO2, Nyasil™) and aminopropyl (-(CH2)3-NH2,) functionalized silica nanoparticles (Stoga) during the synthesis of calcium-silicate-hydrate (C-S-H gel). Characterization by solid state (29)Si NMR and ATR-FTIR spectroscopy showed that the addition of both particle types increases the average length of the silicate chains in C-S-H gel being this effect slightly more important in the case of Stoga particles. In addition, (13)C NMR and XPS confirmed that the aminopropyl chain remains in the final product cleaved to silicon atoms at the end of the silicate chain of C-S-H gel whereas XRD measurements showed that this result in an increment in the basal distance compared with ordinary CSH. In addition, the dynamics of water within the pores of C-S-H gel was analyzed by broadband dielectric spectroscopy. We observed that water confined in C-S-H formed with the addition of nanoparticles is faster than that in plain C-S-H which can be related to a different porous structure in these materials.

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Metadata

Authors
Monasterio, M., Gaitero, J. J., Erkizia, E., Guerrero Bustos, A. M., Miccio, L. A., Dolado, J. S., & Cerveny, S.
Affiliations
  • Material Physics Center (ES)
  • Euskadiko Parke Teknologikoa (ES)
Corresponding author
Cerveny, Silvina
ORCID
Venue
Journal of Colloid and Interface Science
Publisher
Elsevier BV
Published
2015-07
Volume
450
Pages
109-118
ISSN
0021-9797 (ISSN-L)
DOI
10.1016/j.jcis.2015.02.066
OpenAlex
W2022960312
Cited by
106
References
0
Citations by year
2026: 9 · 2025: 11 · 2024: 17 · 2023: 11 · 2022: 6 · 2021: 12 · 2020: 13 · 2019: 7 · 2018: 7 · 2017: 10 · 2016: 1 · 2015: 2
FWCI
10.31
Type
journal article
Language
en
Open access
closed
Licence
www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations
  • Journal of Colloid and Interface Science (publishedVersion)
  • PubMed (publishedVersion)
  • DIGITAL.CSIC (Spanish National Research Council (CSIC)) (submittedVersion)
  • TECNALIA Publications (Fundación TECNALIA Research & Innovation) (submittedVersion, public-domain)
Funders
Basque Government (IE14-393)
Topics
  • Physical Sciences › Engineering › Civil and Structural Engineering › Concrete and Cement Materials Research
  • Physical Sciences › Materials Science › Biomaterials › Calcium Carbonate Crystallization and Inhibition
  • Physical Sciences › Materials Science › Materials Chemistry › Mesoporous Materials and Catalysis
Keywords
calcium silicate hydrate, silica nanoparticles, aminopropyl-functionalized silica, nanoparticle addition, gel microstructure, cement hydration

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CoChat. (2026). Citation check: Effect of addition of silica- and amine functionalized silica-nanoparticles on the microstructure of calcium silicate hydrate (C–S–H) gel. https://app.cochat.ai/papers/10.1016/j.jcis.2015.02.066
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Monasterio, M., Gaitero, J. J., Erkizia, E., Guerrero Bustos, A. M., Miccio, L. A., Dolado, J. S., & Cerveny, S. (2015). Effect of addition of silica- and amine functionalized silica-nanoparticles on the microstructure of calcium silicate hydrate (C–S–H) gel. Journal of Colloid and Interface Science. https://doi.org/10.1016/j.jcis.2015.02.066