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Investigating the solid electrolyte interphase using binder-free graphite electrodes
Open accessAbstract
Abstract Binder-free (BF) electrodes simplify interpretation of solid electrolyte interphase (SEI) data obtained from studies of graphite surfaces. In this work, we prepared BF-graphite electrodes by electrophoretic deposition (EPD), and the SEI layers formed on the electrode in lithium cells containing LiPF6- and LiF2BC2O4-bearing electrolytes were examined by Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS). The results showed that the dominant SEI species were lithium alkyl carbonates (ROCO2Li) and lithium alkoxides (ROLi); Li2CO3 was conspicuously absent. Trigonal borate oligomers are most likely present in the SEI of graphite samples cycled in LiF2BC2O4 electrolyte, while lithium fluorophosphates are present on graphite samples cycled in LiPF6 electrolyte. The SEI layer coverage was greater on graphite samples cycled in LiF2BC2O4 electrolyte than in the LiPF6 electrolyte. Our results demonstrate that BF-graphite electrodes prepared by EPD are suitable for the study of SEI layer formed in various electrolyte systems.
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Cites
An unique lithium salt for the improved electrolyte of Li-ion battery
Shui Zhang, S. (2006) · Electrochemistry Communications · doi:10.1016/j.elecom.2006.06.016 · Cited by 382
Cited by
Electrolytes and Interphases in Li-Ion Batteries and Beyond
Xu, K. (2014) · Chemical Reviews · doi:10.1021/cr500003w · Cited by 5,566
Nie, M., Abraham, D. P., Chen, Y., Bose, A., & Lucht, B. L. (2013) · The Journal of Physical Chemistry C · doi:10.1021/jp404155y · Cited by 578
Self-citationIdentifying the components of the solid–electrolyte interphase in Li-ion batteries
Wang, L., Menakath, A., Han, F., Wang, Y., Zavalij, P. Y., Gaskell, K. J., Borodin, O., Iuga, D., Brown, S. P., Wang, C., et al. (2019) · Nature Chemistry · doi:10.1038/s41557-019-0304-z · Cited by 514
Effects of inhomogeneities - nanoscale to mesoscale - on the durability of Li-Ion batteries
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Metadata
- Authors
- Kang, S.-H., Abraham, D. P., Xiao, A., & Lucht, B. L.
- Venue
- Journal of Power Sources
- Publisher
- Elsevier BV
- Published
- 2008-01
- Volume
- 175
- Issue
- 1
- Pages
- 526-532
- ISSN
- 0378-7753 (ISSN-L)
- OpenAlex
- W2072427727
- Cited by
- 172
- References
- 1
- FWCI
- 2.83
- Type
- journal article
- Language
- en
- Open access
- green
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- Kang, S.-H., Abraham, D. P., Xiao, A., & Lucht, B. L. (2008). Investigating the solid electrolyte interphase using binder-free graphite electrodes. Journal of Power Sources. https://doi.org/10.1016/j.jpowsour.2007.08.112
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