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Structural characterization of phase transition of Al2O3 nanopowders obtained by polymeric precursor method
Open accessAbstract
Nanocrystalline Al2O3powders have been synthesized by the polymeric precursor method. A study of the evolution of crystalline phases of obtained powders was accomplished through X-ray diffraction, micro-Raman spectroscopy and refinement of the structures through the Rietveld method. The results obtained allow the identification of three steps on the -Al2O3 to -Al2O3 phase transition. The single-phase -Al2O3 powder was obtained after heat-treatment at 1050 ◦ C for 2 h. A study of the morphology of the particles was accomplished through measures of crystallite size, specific surface area and transmission electronic microscopy. The particle size is closely related to -Al2O3 to -Al2O3 phase transition.
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Rietveld refinement of Debye–Scherrer synchrotron X-ray data from Al2O3
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A novel chemical route for the synthesis of nanocrystalline α-Al2O3 powder
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Pan, Z., Yao, L., Zhai, J., Fu, D., Shen, B., & Wang, H. (2017) · ACS Applied Materials & Interfaces · doi:10.1021/acsami.6b13663 · Cited by 267
Ismail, R. A., Zaidan, S. A., & Kadhim, R. M. (2017) · Applied Nanoscience · doi:10.1007/s13204-017-0580-0 · Cited by 89
Heredia, A., Gómez Avila, J., Vinuesa, A., Saux, C., Mendoza, S. M., Garay, F., & Crivello, M. (2019) · Adsorption · doi:10.1007/s10450-019-00109-2 · Cited by 18
Metadata
- Authors
- Cava, S., Tebcherani, S. M., Souza, I. A., Pianaro, S. A., Paskocimas, C. A., Longo, E., & Varela, J. A.
- Venue
- Materials Chemistry and Physics
- Publisher
- Elsevier BV
- Published
- 2007-06
- Volume
- 103
- Issue
- 2-3
- Pages
- 394-399
- ISSN
- 0254-0584 (ISSN-L)
- OpenAlex
- W2143802240
- Cited by
- 265
- References
- 8
- FWCI
- 4.61
- Type
- journal article
- Language
- en
- Open access
- green
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- Cava, S., Tebcherani, S. M., Souza, I. A., Pianaro, S. A., Paskocimas, C. A., Longo, E., & Varela, J. A. (2007). Structural characterization of phase transition of Al2O3 nanopowders obtained by polymeric precursor method. Materials Chemistry and Physics. https://doi.org/10.1016/j.matchemphys.2007.02.046
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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