A simple synthesis of ZnO:Co2O3 nanocomposites by pulsed laser irradiation in liquid
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Nanocomposite materials are emerging in popularity due to their enhanced performance over the constituent materials. In this work, we report the fabrication of zinc oxide: cobalt oxide nanocomposites in a simple, fast and room temperature synthesis with good productivity. The nanocomposites synthesized were characterized by SEM, XPS and UV-Visible spectroscopy to analyze their morphology, composition, chemical states, optical absorption, band gap etc. The nanocolloids of the composite were drop casted to form thin films for photocatalytic studies. In SEM analysis, the morphological transformation of the material is observed where it transformed from agglomerated spherical particles to petals shaped and then to partially spherical forms due to pulsed laser irradiation. XPS analysis showed a gradual change in oxygen high resolution spectra in the samples with respect to the concentration difference of cobalt oxide. The optical studies show an enhanced absorption in visible region for the nanocomposite and the energy band gap reduced to 2.4 eV. All the thin films of nanocomposite showed photocatalytic decay of methylene blue dye under visible light irradiation. The results of this study support the effective use of laser irradiation in liquid to obtain nanocomposites of metal oxides for photocatalytic applications.
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ZnO/Co2O3 synthesized by PLI in liquid medium showed enhanced photocatalytic activity against methylene blue dye in water.
“The same research group investigated the facile PLI synthesis of ZnO/Co2O3 in a liquid medium for the enhancement of photocatalytic activity against methylene blue (MB) dye in water154.”
From Fundamentals and comprehensive insights on pulsed laser synthesis of advanced materials for diverse photo- and electrocatalytic applications (2022) · cites this paper as [154]
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Synthesis and characterization of black TiO2 nanoparticles by pulsed laser irradiation in liquid
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Theerthagiri, J., Karuppasamy, K., Lee, S. J., Shwetharani, R., Kim, H.-S., Pasha, S. K. K., Ashokkumar, M., & Choi, M. Y. (2022) · Light: Science & Applications · doi:10.1038/s41377-022-00904-7 · Cited by 461 · see citing works
- Authors
- Kanakkillam, S. S., Krishnan, B., Avellaneda, D. A., & Shaji, S.
- Affiliations
- Universidad Autónoma de Nuevo León (MX)
- Corresponding author
- Shaji, Sadasivan
- Venue
- Materials Today: Proceedings
- Publisher
- Elsevier BV
- Published
- 2020
- Volume
- 33
- Pages
- 1444-1452
- ISSN
- 2214-7853 (ISSN-L)
- PMC
- PMC7513878
- OpenAlex
- W3088175719
- Cited by
- 10
- References
- 1
- Citations by year
- 2026: 2 · 2025: 1 · 2024: 4 · 2022: 1 · 2021: 2
- FWCI
- 0.29
- Type
- journal article
- Language
- en
- Open access
- green
- www.ncbi.nlm.nih.gov
- Locations
- Materials Today Proceedings (publishedVersion)
- PubMed Central (publishedVersion)
- PubMed (publishedVersion)
- El Repositorio Academico Digital de la UANL (Universidad Autónoma de Nuevo León) (submittedVersion)
- Funders
- Consejo Nacional de Ciencia y Tecnología
- Universidad Autónoma de Nuevo León
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › ZnO doping and properties
- Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Advanced Photocatalysis Techniques
- Physical Sciences › Engineering › Biomedical Engineering › Laser-Ablation Synthesis of Nanoparticles
- Keywords
- zinc oxide, cobalt oxide, room-temperature synthesis, metal oxide nanocomposites, nanocolloids, thin films, photocatalytic degradation, methylene blue, visible light photocatalysis, band gap narrowing, optical absorption, morphological transformation
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