Confined crystallization phenomena in immiscible polymer blends with dispersed micro-and nanometer sized PA6 droplets, part 2: reactively compatibilized PS/PA6 and (PPE/PS)/PA6 blends
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Adding a compatibilizer is an effective way to tailor the dispersed phase size in immiscible blends.
“In fact, besides tuning the composition, adding a compatibilizer is known as an effective way to tailor the dispersed phase size.”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [32]
In PS/PA6 75/25 blends reactively compatibilized with SMA2, without compatibilizer fractionated crystallization shows two main peaks at 188°C and around 170°C from droplets of average size around 2 μm; adding SMA2 causes a low-temperature exotherm around 95°C and decreases high-temperature fractionated peaks; above about 5-6% SMA2, morphology with average droplet size below 0.2 μm does not change,
“PS/PA6 blend without compatibilizer exhibits fractionated crystallization with two main peaks: one at the bulk crystallization temperature (188 °C), and the second at around 170 °C.This fractionated crystallization is the result of a droplet dispersion with an average size of around 2 μm.The addition of SMA2 has a noteworthy effect, causing the appearance of a low-temperature exotherm, located”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [32]
The origin of fractionated crystallization is the lack of efficient nuclei.
“The origin of fractionated crystallization is ascribed to the lack of efficient nuclei, and this hypothesis can also be verified by the addition of nucleating agents.[ 8 , 13 , 32 , 46 , 4 8 , 4 9 ]”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [32]
Addition of nucleating agents can verify the hypothesis that fractionated crystallization originates from a lack of efficient nuclei.
“The origin of fractionated crystallization is ascribed to the lack of efficient nuclei, and this hypothesis can also be verified by the addition of nucleating agents.[ 8 , 13 , 32 , 46 , 4 8 , 4 9 ]”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [32]
With addition of talc to PA6/PS blends, the exothermic enthalpy of the higher crystallization peak increased at the expense of that of the lower crystallization peak.
“With the addition of talc, the exothermic enthalpy of the higher crystallization peak increased at the expense of that of the lower crystallization peak.”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [32]
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References 41 · Cited by 80
- Authors
- Tol, R. T., Mathot, V. B. F., & Groeninckx, G.
- Affiliations
- KU Leuven (BE)
- Corresponding author
- Groeninckx, G.
- ORCID
- Mathot, V.B.F.
- Venue
- Polymer
- Publisher
- Elsevier BV
- Published
- 2005-01
- Volume
- 46
- Issue
- 2
- Pages
- 383-396
- ISSN
- 0032-3861 (ISSN-L)
- OpenAlex
- W2071466293
- Cited by
- 80
- References
- 41
- Citations by year
- 2025: 1 · 2022: 4 · 2021: 3 · 2020: 6 · 2019: 5 · 2018: 6 · 2017: 6 · 2016: 3 · 2015: 3 · 2014: 5 · 2013: 10 · 2012: 2
- FWCI
- 4.95
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Polymer (publishedVersion)
- Topics
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer crystallization and properties
- Physical Sciences › Materials Science › Biomaterials › biodegradable polymer synthesis and properties
- Physical Sciences › Materials Science › Materials Chemistry › Block Copolymer Self-Assembly
- Keywords
- confined crystallization, fractional crystallization, immiscible polymer blends, polyamide 6, polystyrene, reactive compatibilization, compatibilizer, droplet size, heterogeneous nucleation, nucleating agents, supercooling
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