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On the homogeneity of high entropy oxides: An investigation at the atomic scale
Abstract
Abstract Homogeneous distribution of the constituent elements at the atomic scale in high entropy oxides (HEOs) was demonstrated for the first time by atom probe tomography (APT). Three different single-phase HEOs having rocksalt, fluorite, and perovskite type crystal structures were synthesized using nebulized spray pyrolysis process. The as-synthesized powders were compacted into pellets under high pressure of 6 GPa. Both as-synthesized and compacted powders were investigated by X-ray diffraction and transmission electron microscopy. APT results showed that the constituent cations in all three HEO systems were homogenously distributed with no significant segregation or concentration fluctuation even at the atomic scale.
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Cites
Charging Effects on Bonding and Catalyzed Oxidation of CO on Au 8 Clusters on MgO
Yoon, B., Häkkinen, H., Landman, U., Wörz, A. S., Antonietti, J.-M., Abbet, S., Judai, K., & Heiz, U. (2005) · Science · doi:10.1126/science.1104168 · Cited by 1,430
Cited by
Oses, C., Toher, C., & Curtarolo, S. (2020) · Nature Reviews Materials · doi:10.1038/s41578-019-0170-8 · Cited by 2,081
Review of high entropy ceramics: design, synthesis, structure and properties
Zhang, R.-Z., & Reece, M. J. (2019) · Journal of Materials Chemistry A · doi:10.1039/c9ta05698j · Cited by 760
Understanding the Role of Entropy in High Entropy Oxides
Aamlid, S. S., Oudah, M., Rottler, J., & Hallas, A. M. (2023) · Journal of the American Chemical Society · doi:10.1021/jacs.2c11608 · Cited by 574
High entropy oxides: The role of entropy, enthalpy and synergy
Sarkar, A., Breitung, B., & Hahn, H. (2020) · Scripta Materialia · doi:10.1016/j.scriptamat.2020.05.019 · Cited by 389
Self-citationMusicó, B. L., Gilbert, D., Ward, T. Z., Page, K., George, E., Yan, J., Mandrus, D., & Keppens, V. (2020) · APL Materials · doi:10.1063/5.0003149 · Cited by 299
Metadata
- Authors
- Chellali, M. R., Sarkar, A., Nandam, S. H., Bhattacharya, S. S., Breitung, B., Hahn, H., & Velasco, L.
- Venue
- Scripta Materialia
- Publisher
- Elsevier BV
- Published
- 2019-06
- Volume
- 166
- Pages
- 58-63
- ISSN
- 1359-6462 (ISSN-L)
- OpenAlex
- W2920834558
- Cited by
- 159
- References
- 1
- FWCI
- 8.79
- Type
- journal article
- Language
- en
- Open access
- closed
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- Chellali, M. R., Sarkar, A., Nandam, S. H., Bhattacharya, S. S., Breitung, B., Hahn, H., & Velasco, L. (2019). On the homogeneity of high entropy oxides: An investigation at the atomic scale. Scripta Materialia. https://doi.org/10.1016/j.scriptamat.2019.02.039
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