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XRD-based quantitative analysis of clay minerals using reference intensity ratios, mineral intensity factors, Rietveld, and full pattern summation methods: A critical review
Open accessAbstract
The quantification of clay minerals is essential for the evaluation of clay-rich rock and soil, but it remains challenging due to the unique structures and various element compositions of clay minerals. In this article, several quantification methods for clay minerals sourced from X-ray diffraction (XRD) analysis, mainly recommending the reference intensity ratio (RIR), mineral intensity factor (MIF), Rietveld, and full pattern summation methods are reviewed. Principles and applications of these methods are focused upon in addition to related differences in the analysis of clay minerals (i.e., sample preparation, the selection of characteristic reflections for quantification and standards added during analysis). This critical review also provides a proposal for selection of an adaptive XRD quantification method to be applied to various clay-rich samples.
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Cites
Scrivener, K. L., Füllmann, T., Gallucci, E., Walenta, G., & Bermejo, E. (2004) · Cement and Concrete Research · doi:10.1016/j.cemconres.2004.04.014 · Cited by 565
Gualtieri, M. L., Gualtieri, A. F., Gagliardi, S., Ruffini, P., Ferrari, R., & Hanuskova, M. (2010) · Applied Clay Science · doi:10.1016/j.clay.2010.06.002 · Cited by 140
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Low temperature carbonation and CO2 mineral trapping in altered hydrotalcite-rich ultrmafic rocks
Leila, M., Hazlett, R., George, P.-M., Šegvić, B., & Fustic, M. (2025) · Scientific Reports · doi:10.1038/s41598-025-16025-1 · Cited by 16
“XRD analysis was performed on the powdered rock using SmartLAb (Rigaku) equipment following the analytical procedure described by Zhou et al. 48 .”
Toward a Quantitative Understanding of Crystal-Phase Engineering of Ru Nanocrystals
Lin, J.-T., Liu, Y.-H., Tsao, C.-Y., Wu, C.-Y., Hsieh, C.-J., Chen, M.-Z., Chang, C.-W., Hsiao, Y.-C., Chen, H.-L., & Yang, T.-H. (2023) · Chemistry of Materials · doi:10.1021/acs.chemmater.3c00326 · Cited by 15
Metadata
- Authors
- Zhou, X., Liu, D., Bu, H., Deng, L., Liu, H., Yuan, P., Du, P., & Song, H.
- Venue
- Solid Earth Sciences
- Publisher
- Elsevier BV
- Published
- 2018-03
- Volume
- 3
- Issue
- 1
- Pages
- 16-29
- ISSN
- 2451-912X (ISSN-L)
- OpenAlex
- W2784125801
- Cited by
- 323
- References
- 2
- FWCI
- 10.30
- Type
- journal article
- Language
- en
- Open access
- gold
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- The paper
- Zhou, X., Liu, D., Bu, H., Deng, L., Liu, H., Yuan, P., Du, P., & Song, H. (2018). XRD-based quantitative analysis of clay minerals using reference intensity ratios, mineral intensity factors, Rietveld, and full pattern summation methods: A critical review. Solid Earth Sciences. https://doi.org/10.1016/j.sesci.2017.12.002
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