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Sequential Pore Wall Modification in a Covalent Organic Framework for Application in Lactic Acid Adsorption
Open accessAbstract
Abstract Here we describe the synthesis and postsynthetic modification of the stable β-ketoenamine TpBD(NH2)2 covalent organic framework (COF), having primary amine groups integrated into the pore walls. For this purpose we initially synthesized the nitro version of this COF, TpBD(NO2)2. Afterward, TpBD(NO2)2 was reduced to afford the desired framework having primary amine functionality. We demonstrate the accessibility of the primary amine groups and the robustness of the framework by a second modification step, the aminolysis of acetic anhydride, to obtain the corresponding amide form TpBD(NHCOCH3)2. Taking advantage of the high stability of these frameworks under acidic conditions, we study the liquid-phase adsorption of lactic acid, revealing the strong impact of a pore wall modification on the adsorption performance.
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Cites
Tailored crystalline microporous materials by post-synthesis modification
Valtchev, V., Majano, G., Mintova, S., & Pérez-Ramírez, J. (2013) · Chem. Soc. Rev. · doi:10.1039/c2cs35196j · Cited by 478
Cited by
Liu, R., Tan, K. T., Gong, Y., Chen, Y., Li, Z., Xie, S., He, T., Lu, Z., Yang, H., & Jiang, D. (2021) · Chemical Society Reviews · doi:10.1039/d0cs00620c · Cited by 1,083
Wang, H., Zeng, Z., Xu, P., Li, L., Zeng, G., Xiao, R., Tang, Z., Huang, D., Tang, L., Lai, C., et al. (2019) · Chemical Society Reviews · doi:10.1039/c8cs00376a · Cited by 804
Mitra, S., Sasmal, H. S., Kundu, T., Kandambeth, S., Illath, K., Díaz Díaz, D., & Banerjee, R. (2017) · Journal of the American Chemical Society · doi:10.1021/jacs.7b00925 · Cited by 587
Beuerle, F., & Gole, B. (2018) · Angewandte Chemie International Edition · doi:10.1002/anie.201710190 · Cited by 528
Metadata
- Authors
- Lohse, M. S., Stassin, T., Naudin, G., Wuttke, S., Ameloot, R., De Vos, D., Medina, D. D., & Bein, T.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2016-01-04
- Volume
- 28
- Issue
- 2
- Pages
- 626-631
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2317592737
- Cited by
- 233
- References
- 1
- FWCI
- 6.66
- Type
- journal article
- Language
- en
- Open access
- hybrid
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- The paper
- Lohse, M. S., Stassin, T., Naudin, G., Wuttke, S., Ameloot, R., De Vos, D., Medina, D. D., & Bein, T. (2016). Sequential Pore Wall Modification in a Covalent Organic Framework for Application in Lactic Acid Adsorption. Chemistry of Materials. https://doi.org/10.1021/acs.chemmater.5b04388
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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