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Structural Insights and 3D Diffusion Pathways within the Lithium Superionic Conductor Li10GeP2S12
Abstract
Inspired by the ongoing debate about the ion dynamics in the lithium superionic conductor Li 10 GeP 2 S 12 (LGPS), we present neutron powder diffraction data in combination with analyses of differential bond valence and nuclear density maps to elucidate the underlying diffusion pathways in Li 10 GeP 2 S 12 . LGPS exhibits quasi-isotropic three-dimensional lithium diffusion pathways, which is a combination of one-dimensional diffusion channels crossing two diffusion planes. Furthermore, ultrasonic speeds of sound measurements are used to understand the lattice dynamics and obtain the Debye temperature of LGPS. Temperature dependent X-ray diffraction is performed in order to understand the local temperature-dependent behavior of the prevalent structural backbone, as well as the thermal stability of the material. At elevated temperatures, the superionic conducting Li 10 GeP 2 S 12 phase partially decomposes into Li 4 P 2 S 6, explaining the deterioration of the ionic conductivity upon heating.
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Cites
Interface Stability in Solid-State Batteries
Richards, W. D., Miara, L. J., Wang, Y., Kim, J. C., & Ceder, G. (2016) · Chemistry of Materials · doi:10.1021/acs.chemmater.5b04082 · Cited by 1,652
Cited by
Designing solid-state electrolytes for safe, energy-dense batteries
Zhao, Q., Stalin, S., Zhao, C.-Z., & Archer, L. A. (2020) · Nature Reviews Materials · doi:10.1038/s41578-019-0165-5 · Cited by 2,372
Koerver, R., Aygün, I., Leichtweiß, T., Dietrich, C., Zhang, W., Binder, J. O., Hartmann, P., Zeier, W. G., & Janek, J. (2017) · Chemistry of Materials · doi:10.1021/acs.chemmater.7b00931 · Cited by 1,020
Self-citationKoerver, R., Zhang, W., de Biasi, L., Schweidler, S., Kondrakov, A. O., Kolling, S., Brezesinski, T., Hartmann, P., Zeier, W. G., & Janek, J. (2018) · Energy & Environmental Science · doi:10.1039/c8ee00907d · Cited by 872
Self-citationKraft, M. A., Culver, S. P., Calderon, M., Böcher, F., Krauskopf, T., Senyshyn, A., Dietrich, C., Zevalkink, A., Janek, J., & Zeier, W. G. (2017) · Journal of the American Chemical Society · doi:10.1021/jacs.7b06327 · Cited by 760
Self-citationSulfide Solid Electrolytes for Lithium Battery Applications
Lau, J., DeBlock, R. H., Butts, D. M., Ashby, D. S., Choi, C. S., & Dunn, B. S. (2018) · Advanced Energy Materials · doi:10.1002/aenm.201800933 · Cited by 678
Metadata
- Authors
- Weber, D. A., Senyshyn, A., Weldert, K. S., Wenzel, S., Zhang, W., Kaiser, R., Berendts, S., Janek, J., & Zeier, W. G.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2016-08-10
- Volume
- 28
- Issue
- 16
- Pages
- 5905-5915
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2487511233
- Cited by
- 215
- References
- 1
- FWCI
- 10.82
- Type
- journal article
- Language
- en
- Open access
- closed
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- Weber, D. A., Senyshyn, A., Weldert, K. S., Wenzel, S., Zhang, W., Kaiser, R., Berendts, S., Janek, J., & Zeier, W. G. (2016). Structural Insights and 3D Diffusion Pathways within the Lithium Superionic Conductor Li10GeP2S12. Chemistry of Materials. https://doi.org/10.1021/acs.chemmater.6b02424
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