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A Modulated Hydrothermal (MHT) Approach for the Facile Synthesis of UiO-66-Type MOFs
Abstract
Developing a general and economically viable approach for the large-scale synthesis of water-stable metal-organic frameworks (MOFs) with repeatable quality remains the key step for their massive production and commercialization. We herein report a green (aqueous solutions), mild (100 °C, 1 atm), and scalable (can be up to kilograms) modulated hydrothermal (MHT) synthesis of UiO-66, an iconic MOF that has been widely studied recently for its high water stability. More importantly, the MHT synthetic approach can be applied to synthesize other water-stable MOFs with structures identical to UiO-66, such as UiO-66-(F)4, UiO-66-(OCH2CH3)2, and UiO-66-(COOH)4, which cannot be obtained via the traditional solvothermal method. Their performance in postcombustion CO2 capture has also been evaluated. Our MHT approach has clearly depicted a roadmap for the facile synthesis of zirconium-based water stable MOFs to facilitate their massive production and commercialization.
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Cited by
Winarta, J., Shan, B., Mcintyre, S. M., Ye, L., Wang, C., Liu, J., & Mu, B. (2020) · Crystal Growth & Design · doi:10.1021/acs.cgd.9b00955 · Cited by 641
Metal–Organic Frameworks for Food Safety
Wang, P.-L., Xie, L.-H., Joseph, E. A., Li, J.-R., Su, X.-O., & Zhou, H.-C. (2019) · Chemical Reviews · doi:10.1021/acs.chemrev.9b00257 · Cited by 533
Advanced Porous Materials in Mixed Matrix Membranes
Cheng, Y., Ying, Y., Japip, S., Jiang, S., Chung, T., Zhang, S., & Zhao, D. (2018) · Advanced Materials · doi:10.1002/adma.201802401 · Cited by 448
Self-citationMetal-organic frameworks: Challenges and opportunities for ion-exchange/sorption applications
Kumar, P., Pournara, A., Kim, K.-H., Bansal, V., Rapti, S., & Manos, M. J. (2017) · Progress in Materials Science · doi:10.1016/j.pmatsci.2017.01.002 · Cited by 423
When defects turn into virtues: The curious case of zirconium-based metal-organic frameworks
Taddei, M. (2017) · Coordination Chemistry Reviews · doi:10.1016/j.ccr.2017.04.010 · Cited by 341
Metadata
- Authors
- Hu, Z., Peng, Y., Kang, Z., Qian, Y., & Zhao, D.
- Venue
- Inorganic Chemistry
- Publisher
- American Chemical Society (ACS)
- Published
- 2015-05-01
- Volume
- 54
- Issue
- 10
- Pages
- 4862-4868
- ISSN
- 0020-1669 (ISSN-L)
- 1520-510X
- OpenAlex
- W2060111616
- Cited by
- 436
- References
- 0
- FWCI
- 12.54
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: A Modulated Hydrothermal (MHT) Approach for the Facile Synthesis of UiO-66-Type MOFs. https://app.cochat.ai/papers/10.1021/acs.inorgchem.5b00435
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- Hu, Z., Peng, Y., Kang, Z., Qian, Y., & Zhao, D. (2015). A Modulated Hydrothermal (MHT) Approach for the Facile Synthesis of UiO-66-Type MOFs. Inorganic Chemistry. https://doi.org/10.1021/acs.inorgchem.5b00435
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