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ABA Triblock Brush Polymers: Synthesis, Self-Assembly, Conductivity, and Rheological Properties
Open accessAbstract
The synthesis, self-assembly, conductivity, and rheological properties of ABA triblock brush polymers (BBCPs) with grafted polystyrene (A block, N PS = 21) and poly(ethylene oxide) (B block, N PEO = 45) side chains are reported. Two backbone molecular weights ( N A: N B: N A = 11:78:11 and 15:119:15) were investigated with lithium bis(trifluoromethane)sulfonimide (LiTFSI) doping ratios 2 ≤ [EO]:[Li + ] ≤ 20. Blends with 2 ≤ [EO]:[Li + ] ≤ 10 suppress PEO crystallization and self-assemble into hexagonally packed cylinders of the minority g PS component. Conductivity is on the order of 10 –3 S/cm at 105 °C with a corresponding elastic modulus ca. 10 4 Pa. The optimum conductivity occurs at a blend ratio near 10:1 [EO]:[Li + ], similar to that reported for linear block copolymer analogues.
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Fetters, L. J., Lohse, D. J., Richter, D., Witten, T. A., & Zirkel, A. (1994) · Macromolecules · doi:10.1021/ma00095a001 · Cited by 1,999
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Bates, C. M., & Bates, F. S. (2017) · Macromolecules · doi:10.1021/acs.macromol.6b02355 · Cited by 788
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Metadata
- Authors
- Bates, C. M., Chang, A. B., Momčilović, N., Jones, S. C., & Grubbs, R. H.
- Venue
- Macromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 2015-07-07
- Volume
- 48
- Issue
- 14
- Pages
- 4967-4973
- ISSN
- 0024-9297 (ISSN-L)
- 1520-5835
- OpenAlex
- W909557875
- Cited by
- 191
- References
- 1
- FWCI
- 7.38
- Type
- journal article
- Language
- en
- Open access
- green
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- Bates, C. M., Chang, A. B., Momčilović, N., Jones, S. C., & Grubbs, R. H. (2015). ABA Triblock Brush Polymers: Synthesis, Self-Assembly, Conductivity, and Rheological Properties. Macromolecules. https://doi.org/10.1021/acs.macromol.5b00880
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