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Facile Synthesis of BaTiO3 Nanotubes and Their Microwave Absorption Properties

Zhu, Yao-Feng, Zhang, Li, Natsuki, Toshiaki, Fu, Ya-Qin, Ni, Qing-Qing·2012·ACS Applied Materials & Interfaces

Abstract

Uniform BaTiO(3) nanotubes were synthesized via a simple wet chemical route at low temperature (50 °C). The as-synthesized BaTiO(3) nanotubes were characterized using powder X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, Raman spectroscopy, and X-ray photoelectron spectroscopy. The results show that the BaTiO(3) nanotubes formed a cubic phase with an average diameter of ~10 nm and wall thickness of 3 nm at room temperature. The composition of the mixed solvent (ethanol and deionized water) was a key factor in the formation of these nanotubes; we discuss possible synthetic mechanisms. The microwave absorption properties of the BaTiO(3) nanotubes were studied at microwave frequencies between 0.5 and 15 GHz. The minimum reflection loss of the BaTiO(3) nanotubes/paraffin wax composite (BaTiO(3) nanotubes weight fraction = 70%) reached 21.8 dB (~99.99% absorption) at 15 GHz, and the frequency bandwidth less than -10 dB is from 13.3 to 15 GHz. The excellent absorption property of BaTiO(3) nanotubes at high frequency indicates that these nanotubes could be promising microwave-absorbing materials.

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Metadata

Authors
Zhu, Y.-F., Zhang, L., Natsuki, T., Fu, Y.-Q., & Ni, Q.-Q.
Venue
ACS Applied Materials & Interfaces
Published
2012-03-21
Volume
4
Issue
4
Pages
2101-2106
ISSN
  • 1944-8244 (ISSN-L)
  • 1944-8252
OpenAlex
W2428639288
Cited by
180
References
1
FWCI
5.22
Type
journal article
Language
en
Open access
closed

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