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Rapid Microwave-Assisted Green Synthesis of 3D Hierarchical Flower-Shaped NiCo2O4Microsphere for High-Performance Supercapacitor
Abstract
Binary metal oxides with three-dimensional (3D) superstructure have been regarded as desirable electrode materials for the supercapacitor due to the combination of the improved electrical conductivity and effective porous structure. 3D hierarchical flower-shaped nickel cobaltite (NiCo2O4) microspheres have been fabricated by a rapid and template-free microwave-assisted heating (MAH) reflux approach followed by pyrolysis of the as-prepared precursors. The flower-shaped NiCo2O4 microspheres, composed of ultrathin nanopetals with thickness of about 15 nm, are endowed with large specific surface area (148.5 m(2) g(-1)) and a narrow pore size distribution (5-10 nm). The as-fabricated porous flower-shaped NiCo2O4 microspheres as electrode materials for supercapacitor exhibited high specific capacitance of 1006 F g(-1) at 1 A g(-1), enhanced rate capability, and excellent electrochemical stability with 93.2% retention after 1000 continuous charge-discharge (CD) cycles even at a high current density of 8 A g(-1). The desirable integrated performance enables it to be a promising electrode material for the electrochemical supercapacitor (EC).
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Cites
Zhong, J.-H., Wang, A.-L., Li, G.-R., Wang, J.-W., Ou, Y.-N., & Tong, Y.-X. (2012) · Journal of Materials Chemistry · doi:10.1039/c2jm15863a · Cited by 510
Cited by
Moosavifard, S. E., El-Kady, M. F., Rahmanifar, M. S., Kaner, R. B., & Mousavi, M. F. (2015) · ACS Applied Materials & Interfaces · doi:10.1021/am508816t · Cited by 409
Zhang, W., Quan, B., Lee, C., Park, S.-K., Li, X., Choi, E., Diao, G., & Piao, Y. (2015) · ACS Applied Materials & Interfaces · doi:10.1021/am507014w · Cited by 288
Metadata
- Authors
- Lei, Y., Li, J., Wang, Y., Gu, L., Chang, Y., Yuan, H., & Xiao, D.
- Venue
- ACS Applied Materials & Interfaces
- Publisher
- American Chemical Society (ACS)
- Published
- 2014-01-30
- Volume
- 6
- Issue
- 3
- Pages
- 1773-1780
- ISSN
- 1944-8244 (ISSN-L)
- 1944-8252
- OpenAlex
- W2323267917
- Cited by
- 540
- References
- 1
- FWCI
- 22.22
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: Rapid Microwave-Assisted Green Synthesis of 3D Hierarchical Flower-Shaped NiCo2O4Microsphere for High-Performance Supercapacitor. https://app.cochat.ai/papers/10.1021/am404765y
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- Lei, Y., Li, J., Wang, Y., Gu, L., Chang, Y., Yuan, H., & Xiao, D. (2014). Rapid Microwave-Assisted Green Synthesis of 3D Hierarchical Flower-Shaped NiCo2O4Microsphere for High-Performance Supercapacitor. ACS Applied Materials & Interfaces. https://doi.org/10.1021/am404765y
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