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Synthesis of Chitosan-Stabilized Gold Nanoparticles in the Absence/Presence of Tripolyphosphate
Abstract
Gold nanoparticles were prepared by reducing gold salt with a polysaccharide, chitosan, in the absence/presence of tripolyphosphate (TPP). Here, chitosan acted as a reducing/stabilizing agent. The obtained gold nanoparticles were characterized with UV--vis spectroscopy and transmission electron microscopy. The results indicated that the shape and size distribution of gold nanoparticles changed with the molecular weight and concentration of chitosan. More interestingly, the gelation of chitosan upon contacting with polyanion (TPP) can also affect the shape and size distribution of gold nanoparticles. By adding TPP to chitosan solution before the reduction of gold salt, gold nanoparticles have a bimodal size distribution, and at the same time, polygonal gold particles were obtained in addition to spherical gold nanoparticles.
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Kabashin, A. V., Meunier, M., Kingston, C., & Luong, J. H. T. (2003) · The Journal of Physical Chemistry B · doi:10.1021/jp034345q · Cited by 244
Cited by
State of the art in gold nanoparticle synthesis
Zhao, P., Li, N., & Astruc, D. (2013) · Coordination Chemistry Reviews · doi:10.1016/j.ccr.2012.09.002 · Cited by 964
Facile synthesis of Ag and Au nanoparticles utilizing chitosan as a mediator agent
Wei, D., & Qian, W. (2008) · Colloids and Surfaces B: Biointerfaces · doi:10.1016/j.colsurfb.2007.09.030 · Cited by 310
Huang, K.-J., Niu, D.-J., Xie, W.-Z., & Wang, W. (2010) · Analytica Chimica Acta · doi:10.1016/j.aca.2009.11.023 · Cited by 261
Potara, M., Gabudean, A.-M., & Astilean, S. (2011) · Journal of Materials Chemistry · doi:10.1039/c0jm03329d · Cited by 143
Metadata
- Authors
- Huang, H., & Yang, X.
- Venue
- Biomacromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-09-03
- Volume
- 5
- Issue
- 6
- Pages
- 2340-2346
- ISSN
- 1525-7797 (ISSN-L)
- 1526-4602
- OpenAlex
- W2081512722
- Cited by
- 414
- References
- 1
- FWCI
- 4.56
- Type
- journal article
- Language
- en
- Open access
- closed
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