The DOI matches its Crossref record; 8 of the 8 references it cites were found in a registry or an index.
The Shape and Size Distribution of Crystalline Nanoparticles Prepared by Acid Hydrolysis of Native Cellulose
Abstract
The shape and size distribution of crystalline nanoparticles resulting from the sulfuric acid hydrolysis of cellulose from cotton, Avicel, and tunicate were investigated using transmission electron microscopy (TEM) and atomic force microscopy (AFM) as well as small- and wide-angle X-ray scattering (SAXS and WAXS). Images of negatively stained and cryo-TEM specimens showed that the majority of cellulose particles were flat objects constituted by elementary crystallites whose lateral adhesion was resistant against hydrolysis and sonication treatments. Moreover, tunicin whiskers were described as twisted ribbons with an estimated pitch of 2.4-3.2 microm. Length and width distributions of all samples were generally well described by log-normal functions, with the exception of tunicin, which had less lateral aggregation. AFM observation confirmed that the thickness of the nanocrystals was almost constant for a given origin and corresponded to the crystallite size measured from peak broadening in WAXS spectra. Experimental SAXS profiles were numerically simulated, combining the dimensions and size distribution functions determined by the various techniques.
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Cites
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Self-citationPolymer nanocomposites reinforced by cellulose whiskers
Favier, V., Chanzy, H., & Cavaille, J. Y. (1995) · Macromolecules · doi:10.1021/ma00122a053 · Cited by 1,149
Effect of microcrystallite preparation conditions on the formation of colloid crystals of cellulose
DONG, X. M., REVOL, J.-F., & GRAY, D. G. (1998) · Cellulose · doi:10.1023/a:1009260511939 · Cited by 1,032
Sugiyama, J., Vuong, R., & Chanzy, H. (1991) · Macromolecules · doi:10.1021/ma00014a033 · Cited by 791
Araki, J., Wada, M., Kuga, S., & Okano, T. (1998) · Colloids and Surfaces A: Physicochemical and Engineering Aspects · doi:10.1016/s0927-7757(98)00404-x · Cited by 769
Combined infrared and electron diffraction study of the polymorphism of native celluloses
Sugiyama, J., Persson, J., & Chanzy, H. (1991) · Macromolecules · doi:10.1021/ma00009a050 · Cited by 541
Heux, L., Chauve, G., & Bonini, C. (2000) · Langmuir · doi:10.1021/la9913957 · Cited by 467
Self-citationOn the polarity of cellulose in the cell wall of Valonia
Sugiyama, J., Chanzy, H., & Revol, J. (1994) · Planta · doi:10.1007/bf00192539 · Cited by 43
Cited by
Cellulose nanomaterials review: structure, properties and nanocomposites
Moon, R. J., Martini, A., Nairn, J., Simonsen, J., & Youngblood, J. (2011) · Chemical Society Reviews · doi:10.1039/c0cs00108b · Cited by 6,756
Cellulose nanocrystals: chemistry, self-assembly, and applications
Habibi, Y., Lucia, L. A., & Rojas, O. J. (2010) · Chemical Reviews · doi:10.1021/cr900339w · Cited by 5,980
Polylactide (PLA)-based nanocomposites
Raquez, J.-M., Habibi, Y., Murariu, M., & Dubois, P. (2013) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2013.05.014 · Cited by 1,209
Production of nanocrystalline cellulose from lignocellulosic biomass: Technology and applications
Brinchi, L., Cotana, F., Fortunati, E., & Kenny, J. M. (2013) · Carbohydrate Polymers · doi:10.1016/j.carbpol.2013.01.033 · Cited by 1,121
Rosa, M. F., Medeiros, E. S., Malmonge, J. A., Gregorski, K. S., Wood, D. F., Mattoso, L. H. C., Glenn, G., Orts, W. J., & Imam, S. H. (2010) · Carbohydrate Polymers · doi:10.1016/j.carbpol.2010.01.059 · Cited by 1,099
Metadata
- Authors
- Elazzouzi-Hafraoui, S., Nishiyama, Y., Putaux, J.-L., Heux, L., Dubreuil, F., & Rochas, C.
- Venue
- Biomacromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-12-04
- Volume
- 9
- Issue
- 1
- Pages
- 57-65
- ISSN
- 1525-7797 (ISSN-L)
- 1526-4602
- OpenAlex
- W1993035639
- Cited by
- 1,182
- References
- 8
- FWCI
- 8.84
- Type
- journal article
- Language
- en
- Open access
- closed
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