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Controlled Synthesis and Self-Assembly of Single-Crystalline CuO Nanorods and Nanoribbons
Abstract
We report several wet-chemical methods for synthesis of one-dimensional CuO nanostructures in water−ethanol mixed solvents at 77−82 °C and 1 atm. Single-crystalline monodispersed CuO nanorods with a selected breadth in the range of 5−15 nm have been prepared by controlling reagent concentrations. The nanorods are preferentially grown along 〈010〉 directions. A two-step continuous process has also been developed to prepare CuO nanorods and ribbons (length up to 1 μm) with a large aspect ratio under pseudo-steady-state operation. Furthermore, a two-dimensional netted structure has been assembled for the first time from short nanorods formed after prolonged aging; the nanorods are attached each other using their {001}, {100}, and {110} crystal planes. With concentrated NaOH used in synthesis, the nanorods can also be extended along 〈100〉, which gives rise to the formation of CuO nanoplatelets. Various synthetic parameters have also been investigated.
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Cited by
Hydrogen from photo-catalytic water splitting process: A review
Ahmad, H., Kamarudin, S. K., Minggu, L. J., & Kassim, M. (2015) · Renewable and Sustainable Energy Reviews · doi:10.1016/j.rser.2014.10.101 · Cited by 911
Synthetic architecture of interior space for inorganic nanostructures
Zeng, H. C. (2006) · J. Mater. Chem. · doi:10.1039/b511296f · Cited by 462
Self-citationSau, T. K., & Murphy, C. J. (2005) · Langmuir · doi:10.1021/la047488s · Cited by 406
Begildayeva, T., Lee, S. J., Yu, Y., Park, J., Kim, T. H., Theerthagiri, J., Ahn, A., Jung, H. J., & Choi, M. Y. (2021) · Journal of Hazardous Materials · doi:10.1016/j.jhazmat.2020.124412 · Cited by 101
Metadata
- Authors
- Chang, Y., & Zeng, H. C.
- Venue
- Crystal Growth & Design
- Publisher
- American Chemical Society (ACS)
- Published
- 2003-12-03
- Volume
- 4
- Issue
- 2
- Pages
- 397-402
- ISSN
- 1528-7483 (ISSN-L)
- 1528-7505
- OpenAlex
- W2010067671
- Cited by
- 278
- References
- 0
- FWCI
- 5.93
- Type
- journal article
- Language
- en
- Open access
- closed
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