The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
Electrochemical Synthesis of Some Archetypical Zn2+, Cu2+, and Al3+ Metal Organic Frameworks
Abstract
Several archetypical metal organic frameworks (MOFs), namely, HKUST-1, ZIF-8, MIL-100(Al), MIL-53(Al), and NH 2 -MIL-53(Al), were synthesized via anodic dissolution in an electrochemical cell. The influence of different reaction parameters such as solvent, electrolyte, voltage–current density, and temperature on the synthesis yield and textural properties of the MOFs obtained was investigated. The characterization of the samples involved X-ray diffraction, gas adsorption, atomic force microscopy, diffuse reflectance infrared Fourier transform spectroscopy, and scanning electron microscopy. In the present article, we demonstrate that electrochemical synthesis is a robust method offering additional degrees of freedom in the synthesis of these porous materials. The main advantages are the shorter synthesis time, the milder conditions, the facile synthesis of MOF nanoparticles, the morphology tuning and the high Faraday efficiencies. The synthesized MIL-53 and NH 2 -MIL-53 samples exhibit suppressed framework flexibility compared to samples synthesized solvothermally.
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Citations
Cites
An Amine-Functionalized MIL-53 Metal−Organic Framework with Large Separation Power for CO 2 and CH 4
Couck, S., Denayer, J. F. M., Baron, G. V., Rémy, T., Gascon, J., & Kapteijn, F. (2009) · Journal of the American Chemical Society · doi:10.1021/ja900555r · Cited by 988
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Cited by
Metal–organic and covalent organic frameworks as single-site catalysts
Rogge, S. M. J., Bavykina, A., Hajek, J., Garcia, H., Olivos-Suarez, A. I., Sepúlveda-Escribano, A., Vimont, A., Clet, G., Bazin, P., Kapteijn, F., et al. (2017) · Chemical Society Reviews · doi:10.1039/c7cs00033b · Cited by 1,077
Self-citationNew synthetic routes towards MOF production at scale
Rubio-Martinez, M., Avci-Camur, C., Thornton, A. W., Imaz, I., Maspoch, D., & Hill, M. R. (2017) · Chemical Society Reviews · doi:10.1039/c7cs00109f · Cited by 990
Metal Organic Framework Catalysis: Quo vadis?
Gascon, J., Corma, A., Kapteijn, F., & Llabrés i Xamena, F. X. (2014) · ACS Catalysis · doi:10.1021/cs400959k · Cited by 960
Self-citationYusuf, V. F., Malek, N. I., & Kailasa, S. K. (2022) · ACS Omega · doi:10.1021/acsomega.2c05310 · Cited by 894
MOF positioning technology and device fabrication
Falcaro, P., Ricco, R., Doherty, C. M., Liang, K., Hill, A. J., & Styles, M. J. (2014) · Chem. Soc. Rev. · doi:10.1039/c4cs00089g · Cited by 710
Metadata
- Authors
- Martinez Joaristi, A., Juan-Alcañiz, J., Serra-Crespo, P., Kapteijn, F., & Gascon, J.
- Venue
- Crystal Growth & Design
- Publisher
- American Chemical Society (ACS)
- Published
- 2012-06-06
- Volume
- 12
- Issue
- 7
- Pages
- 3489-3498
- ISSN
- 1528-7483 (ISSN-L)
- 1528-7505
- OpenAlex
- W2313713709
- Cited by
- 569
- References
- 1
- FWCI
- 10.49
- Type
- journal article
- Language
- en
- Open access
- closed
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- Martinez Joaristi, A., Juan-Alcañiz, J., Serra-Crespo, P., Kapteijn, F., & Gascon, J. (2012). Electrochemical Synthesis of Some Archetypical Zn2+, Cu2+, and Al3+ Metal Organic Frameworks. Crystal Growth & Design. https://doi.org/10.1021/cg300552w
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