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Preparation of Monodispersed Fe−Mo Nanoparticles as the Catalyst for CVD Synthesis of Carbon Nanotubes
Abstract
Uniform iron−molybdenum nanoparticles were prepared by thermal decomposition of metal carbonyl complexes using a mixture of long-chain carboxylic acid and long-chain amine as protective agents. The sizes of the nanoparticles can be systematically varied from 3 to 14 nm by changing the experimental conditions. High-resolution TEM images and EDX data show that the prepared nanoparticles are highly crystalline iron nanoparticles containing ≈4% molybdenum. The effects of the concentration, reaction time, the ratio of metal carbonyl complexes versus protective agents, and the ratio of acid/amine of the protective agents on the sizes of the produced nanoparticles were systematically studied. The prepared nanoparticles were used as catalysts for single-walled carbon nanotube growth and the results indicate that there is an upper limit for the size of the catalyst particles to nucleate single-walled carbon nanotubes.
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Citations
Cites
Monodisperse FePt Nanoparticles and Ferromagnetic FePt Nanocrystal Superlattices
Sun, S., Murray, C. B., Weller, D., Folks, L., & Moser, A. (2000) · Science · doi:10.1126/science.287.5460.1989 · Cited by 6,137
Cited by
Anantharaj, S., Ede, S. R., Sakthikumar, K., Karthick, K., Mishra, S., & Kundu, S. (2016) · ACS Catalysis · doi:10.1021/acscatal.6b02479 · Cited by 2,503
Devaraj, M., Saravanan, R., Deivasigamani, R., Gupta, V. K., Gracia, F., & Jayadevan, S. (2016) · Journal of Molecular Liquids · doi:10.1016/j.molliq.2016.06.028 · Cited by 382
Controlled Synthesis and Assembly of FePt Nanoparticles
Sun, S., Anders, S., Thomson, T., Baglin, J. E. E., Toney, M. F., Hamann, H. F., Murray, C. B., & Terris, B. D. (2003) · The Journal of Physical Chemistry B · doi:10.1021/jp027314o · Cited by 358
SYNTHESIS ROUTES FOR LARGE VOLUMES OF NANOPARTICLES
Masala, O., & Seshadri, R. (2004) · Annual Review of Materials Research · doi:10.1146/annurev.matsci.34.052803.090949 · Cited by 355
Synthesis Methods of Carbon Nanotubes and Related Materials
Szabó, A., Perri, C., Csató, A., Giordano, G., Vuono, D., & Nagy, J. B. (2010) · Materials · doi:10.3390/ma3053092 · Cited by 339
Metadata
- Authors
- Li, Y., Liu, J., Wang, Y., & Wang, Z. L.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2001-02-06
- Volume
- 13
- Issue
- 3
- Pages
- 1008-1014
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2024657566
- Cited by
- 315
- References
- 1
- FWCI
- 11.59
- Type
- journal article
- Language
- en
- Open access
- closed
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- Li, Y., Liu, J., Wang, Y., & Wang, Z. L. (2001). Preparation of Monodispersed Fe−Mo Nanoparticles as the Catalyst for CVD Synthesis of Carbon Nanotubes. Chemistry of Materials. https://doi.org/10.1021/cm000787s
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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