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Preparation of Size-Controlled TiO2 Nanoparticles and Derivation of Optically Transparent Photocatalytic Films
Abstract
TiO 2 nanoparticles were prepared by hydrothermal reaction of titanium alkoxide stabilized in acidic ethanol/water solution. The sizes of particles have been controlled to the range of 7−25 nm by adjusting the concentration of Ti precursor and the composition of the solvent system. The TiO 2 samples synthesized under this acidic ethanol/water environment were mainly primary particles in anatase phase without secondary structure. The suspension of as-prepared 7-nm-sized TiO 2 nanoparticles demonstrates long-term stability, and has been applied successfully for the fabrication of ultra-transparent particulate TiO 2 films. The photocatalytic efficiency of TiO 2 films prepared from the 7-nm-sized nanoparticles was 1.6 times of that of films derived from Degussa P25 in decomposing gaseous 2-propanol.
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Cites
Environmental applications of semiconductor photocatalysis
Hoffmann, M. R., Martin, S. T., Choi, W., & Bahnemann, D. W. (1995) · Chemical Reviews · doi:10.1021/cr00033a004 · Cited by 18,495
Synthesis of TiO2 Nanocrystals by Nonhydrolytic Solution-Based Reactions
Trentler, T. J., Denler, T. E., Bertone, J. F., Agrawal, A., & Colvin, V. L. (1999) · Journal of the American Chemical Society · doi:10.1021/ja983361b · Cited by 382
Cited by
Titanium Dioxide Nanomaterials: Synthesis, Properties, Modifications, and Applications
Chen, X., & Mao, S. S. (2007) · Chemical Reviews · doi:10.1021/cr0500535 · Cited by 10,688
Semiconductor-based Photocatalytic Hydrogen Generation
Chen, X., Shen, S., Guo, L., & Mao, S. S. (2010) · Chemical Reviews · doi:10.1021/cr1001645 · Cited by 7,876
TiO2 photocatalyst for water treatment applications
Lee, S.-Y., & Park, S.-J. (2013) · Journal of Industrial and Engineering Chemistry · doi:10.1016/j.jiec.2013.07.012 · Cited by 992
Self-citationPreparation of graphene–TiO 2 composites with enhanced photocatalytic activity
Zhou, K., Zhu, Y., Yang, X., Jiang, X., & Li, C. (2011) · New J. Chem. · doi:10.1039/c0nj00623h · Cited by 576
Solution-Phase Synthesis of Titanium Dioxide Nanoparticles and Nanocrystals
Cargnello, M., Gordon, T. R., & Murray, C. B. (2014) · Chemical Reviews · doi:10.1021/cr500170p · Cited by 406
Metadata
- Authors
- Chae, S. Y., Park, M. K., Lee, S. K., Kim, T. Y., Kim, S. K., & Lee, W. I.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2003-07-16
- Volume
- 15
- Issue
- 17
- Pages
- 3326-3331
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2080931034
- Cited by
- 303
- References
- 2
- FWCI
- 4.50
- Type
- journal article
- Language
- en
- Open access
- closed
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- Chae, S. Y., Park, M. K., Lee, S. K., Kim, T. Y., Kim, S. K., & Lee, W. I. (2003). Preparation of Size-Controlled TiO2 Nanoparticles and Derivation of Optically Transparent Photocatalytic Films. Chemistry of Materials. https://doi.org/10.1021/cm030171d
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