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Surface Passivation of Bare Aluminum Nanoparticles Using Perfluoroalkyl Carboxylic Acids
Abstract
Surface passivation of unpassivated Al nanoparticles has been realized using self-assembled monolayers (SAMs). Nanoscale Al particles were prepared in solution by catalytic decomposition of H 3 Al·NMe 3 or H 3 Al·N(Me)Pyr by Ti(O i Pr) 4 and coated in situ using a perfluoroalkyl carboxylic acid SAM. Because the Al particles are prepared using wet chemistry techniques and coated in solution, they are free of oxygen passivation. This SAM coating passivates the aluminum and appears to prevent the oxidation of the particles in air and renders the composite material, to some extent, soluble in polar organic solvents such as diethyl ether. Characterization data including scanning electron microscopy, transmission electron microscopy, thermogravimetric analysis, and attenuated total reflectance-Fourier transform infrared spectroscopy of prepared materials are presented.
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Citations
Cited by
Historical and current usage of per- and polyfluoroalkyl substances (PFAS): A literature review
Gaines, L. G. T. (2023) · American Journal of Industrial Medicine · doi:10.1002/ajim.23362 · Cited by 665
Influence of ligand structure on the stability and oxidation of copper nanoparticles
Kanninen, P., Johans, C., Merta, J., & Kontturi, K. (2008) · Journal of Colloid and Interface Science · doi:10.1016/j.jcis.2007.09.069 · Cited by 289
Aluminum: An underappreciated anode material for lithium-ion batteries
Chang, X., Xie, Z., Liu, Z., Zheng, X., Zheng, J., & Li, X. (2020) · Energy Storage Materials · doi:10.1016/j.ensm.2019.10.027 · Cited by 62
Metadata
- Authors
- Jouet, R. J., Warren, A. D., Rosenberg, D. M., Bellitto, V. J., Park, K., & Zachariah, M. R.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2005-05-01
- Volume
- 17
- Issue
- 11
- Pages
- 2987-2996
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W3158148138
- Cited by
- 232
- References
- 0
- FWCI
- 10.15
- Type
- journal article
- Language
- en
- Open access
- closed
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