The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
Synthesis of Variable-Sized Nanocrystals of Fe3O4 with High Surface Reactivity
Abstract
A new rational method of synthesis of nanocrystalline iron (II, III) oxide is based on the elevated-temperature hydrolysis of chelate iron alkoxide complexes in solutions of corresponding alcohol, diethylene glycol, and N -methyl diethanolamine. The rates of reaction and crystallization are easily tuned by varying the concentration of reactants and changing the temperature. The size of the nanocrystals is controlled by changing the complexing strength of the reaction medium: 5.7 nm in diethylene glycol, 16.8 nm in N -methyl diethanolamine, and 12.7 nm in a 1:1 mixture of both solvents. The nanocrystalline powdered Fe 3 O 4 products were isolated with a high yield. The surface of the obtained nanocrystals is passivated by molecules of adsorbed donating solvent that provide stability against agglomeration, provide solubility in polar protic solvents (water and methanol), and allow reactions at the nanocrystal surface.
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Cites
Synthesis of TiO2 Nanocrystals by Nonhydrolytic Solution-Based Reactions
Trentler, T. J., Denler, T. E., Bertone, J. F., Agrawal, A., & Colvin, V. L. (1999) · Journal of the American Chemical Society · doi:10.1021/ja983361b · Cited by 382
Cited by
Fundamentals and advances in magnetic hyperthermia
Périgo, E. A., Hemery, G., Sandre, O., Ortega, D., Garaio, E., Plazaola, F., & Teran, F. J. (2015) · Applied Physics Reviews · doi:10.1063/1.4935688 · Cited by 836
Badruddoza, A. Z. M., Tay, A. S. H., Tan, P. Y., Hidajat, K., & Uddin, M. S. (2011) · Journal of Hazardous Materials · doi:10.1016/j.jhazmat.2010.10.029 · Cited by 572
Facile synthesis of superparamagnetic magnetite nanoparticles in liquid polyols
Cai, W., & Wan, J. (2007) · Journal of Colloid and Interface Science · doi:10.1016/j.jcis.2006.10.023 · Cited by 481
Solvothermal Synthesis and Characterization of Fe3O4 and γ-Fe2O3 Nanoplates
Lu, J., Jiao, X., Chen, D., & Li, W. (2009) · The Journal of Physical Chemistry C · doi:10.1021/jp810583e · Cited by 308
Studies on the magnetism of cobalt ferrite nanocrystals synthesized by hydrothermal method
Zhao, L., Zhang, H., Xing, Y., Song, S., Yu, S., Shi, W., Guo, X., Yang, J., Lei, Y., & Cao, F. (2008) · Journal of Solid State Chemistry · doi:10.1016/j.jssc.2007.10.034 · Cited by 302
Metadata
- Authors
- Caruntu, D., Caruntu, G., Chen, Y., O'Connor, C. J., Goloverda, G., & Kolesnichenko, V. L.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-11-11
- Volume
- 16
- Issue
- 25
- Pages
- 5527-5534
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2038318684
- Cited by
- 223
- References
- 1
- FWCI
- 7.56
- Type
- journal article
- Language
- en
- Open access
- closed
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
