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Zeolite (MFI) Crystal Morphology Control Using Organic Structure-Directing Agents
Abstract
The effect of structure-directing agents (SDAs) on zeolite particle morphology and crystal structure was studied. Dimers and trimers of tetrapropylammonium hydroxide the SDA of siliceous ZSM-5 (silicalite-1, structure type MFI) lead to direct growth of the same framework but with drastically different crystal morphologies. Control over relative crystal growth rates along the three main crystallographic axes is demonstrated by obtaining crystals with their longest dimension along any of these axes. Unit cell dimensions and crystal structure were determined by refinement based on powder X-ray diffraction data and electron microscopy, respectively. The importance of the new morphologies in thin film molecular sieve technology along with possible crystal growth mechanisms is discussed.
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Cites
On the origins of morphological complexity in block copolymer surfactants
Jain, S., & Bates, F. S. (2003) · Science · doi:10.1126/science.1082193 · Cited by 1,217
Cited by
Ultra-selective high-flux membranes from directly synthesized zeolite nanosheets
Jeon, M. Y., Kim, D., Kumar, P., Lee, P. S., Rangnekar, N., Bai, P., Shete, M., Elyassi, B., Lee, H. S., Narasimharao, K., et al. (2017) · Nature · doi:10.1038/nature21421 · Cited by 574
Self-citationSnyder, M. A., & Tsapatsis, M. (2007) · Angewandte Chemie International Edition · doi:10.1002/anie.200604910 · Cited by 355
Self-citationČejka, J., Centi, G., Perez-Pariente, J., & Roth, W. J. (2012) · Catalysis Today · doi:10.1016/j.cattod.2011.10.006 · Cited by 312
Xu, D., Ma, Y., Jing, Z., Han, L., Singh, B., Feng, J., Shen, X., Cao, F., Oleynikov, P., Sun, H., et al. (2014) · Nature Communications · doi:10.1038/ncomms5262 · Cited by 279
Metadata
- Authors
- Bonilla, G., Díaz, I., Tsapatsis, M., Jeong, H.-K., Lee, Y., & Vlachos, D. G.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-11-26
- Volume
- 16
- Issue
- 26
- Pages
- 5697-5705
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2078757955
- Cited by
- 189
- References
- 1
- FWCI
- 5.76
- Type
- journal article
- Language
- en
- Open access
- closed
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