The DOI matches its Crossref record; 8 of the 8 references it cites were found in a registry or an index.
Functionalization of Nanoscale Diamond Powder: Fluoro-, Alkyl-, Amino-, and Amino Acid-Nanodiamond Derivatives
Abstract
The reaction of nanoscale diamond (ND) powder with an elemental fluorine/hydrogen mixture at temperatures varying from 150 to 470 °C resulted in the high degree of ND surface fluorination yielding a fluoro-nanodiamond with up to 8.6 at. % fluorine content. The fluoro-nanodiamond was used as a precursor for preparation of the series of functionalized nanodiamonds by subsequent reactions with alkyllithium reagents, diamines, and amino acids. The fluoro-nanodiamond and corresponding alkyl-, amino-, and amino acid-nanodiamond derivatives were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transformed infrared (FTIR) and X-ray photoelectron spectroscopy (XPS), and thermal gravimetry-mass spectrometry (TG-MS) measurements. In comparison with the pristine nanodiamond, all functionalized nanodiamonds show an improved solubility in polar organic solvents, e.g., alcohols and THF, and a reduced particle agglomeration. The developed methodology provides an efficient method for the chemical modification of nanodiamond powder, which enables a variety of engineering and biomedical applications of ND derivatives.
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Cites
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Detonation synthesis ultradispersed diamonds: properties and applications
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Fluorination of Single-Wall Carbon Nanotubes and Subsequent Derivatization Reactions
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Self-citationElastic, mechanical, and thermal properties of nanocrystalline diamond films
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Photochemical Modification of Diamond Surfaces
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Cited by
The properties and applications of nanodiamonds
Mochalin, V. N., Shenderova, O., Ho, D., & Gogotsi, Y. (2012) · Nature Nanotechnology · doi:10.1038/nnano.2011.209 · Cited by 2,745
Georgakilas, V., Perman, J. A., Tucek, J., & Zboril, R. (2015) · Chemical Reviews · doi:10.1021/cr500304f · Cited by 2,147
Nanodiamond Particles: Properties and Perspectives for Bioapplications
Schrand, A. M., Hens, S. A. C., & Shenderova, O. A. (2009) · Critical Reviews in Solid State and Materials Sciences · doi:10.1080/10408430902831987 · Cited by 802
New Carbon Materials: Biological Applications of Functionalized Nanodiamond Materials
Krueger, A. (2008) · Chemistry – A European Journal · doi:10.1002/chem.200700987 · Cited by 431
Surface functionalisation of detonation diamond suitable for biological applications
Krüger, A., Liang, Y., Jarre, G., & Stegk, J. (2006) · J. Mater. Chem. · doi:10.1039/b601325b · Cited by 347
Metadata
- Authors
- Liu, Y., Gu, Z., Margrave, J. L., & Khabashesku, V. N.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-09-02
- Volume
- 16
- Issue
- 20
- Pages
- 3924-3930
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2095041821
- Cited by
- 353
- References
- 8
- FWCI
- 7.50
- Type
- journal article
- Language
- en
- Open access
- closed
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