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Highly Crystalline Cubic Mesoporous TiO2 with 10-nm Pore Diameter Made with a New Block Copolymer Template
Abstract
A strategy is shown to fabricate highly organized mesoporous anatase films exhibiting favorable properties for photocatalysis and photovoltaic applications by the hydrolysis/condensation of TiCl 4 in the presence of PHB−PEO block copolymer templates. Dipcoating for evaporation-induced-self-assembly followed by a straight thermal treatment was employed. The evaporation/structuration process and the thermal treatment were mechanistically followed by in situ GISAXS/WAXS measurements, and the final product was carefully analyzed by spectroscopic ellipsometry and transmission electron microscopy to reveal the consequences of crystallization onto the micro-, the meso-, and the macroscale.
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Citations
Cited by
Titanium Dioxide Nanomaterials: Synthesis, Properties, Modifications, and Applications
Chen, X., & Mao, S. S. (2007) · Chemical Reviews · doi:10.1021/cr0500535 · Cited by 10,688
Templated Nanocrystal-Based Porous TiO2 Films for Next-Generation Electrochemical Capacitors
Brezesinski, T., Wang, J., Polleux, J., Dunn, B., & Tolbert, S. H. (2009) · Journal of the American Chemical Society · doi:10.1021/ja8057309 · Cited by 1,076
Self-citationPlasmon Resonant Enhancement of Photocatalytic Water Splitting Under Visible Illumination
Liu, Z., Hou, W., Pavaskar, P., Aykol, M., & Cronin, S. B. (2011) · Nano Letters · doi:10.1021/nl104005n · Cited by 1,011
Ordered mesoporous metal oxides: synthesis and applications
Ren, Y., Ma, Z., & Bruce, P. G. (2012) · Chemical Society Reviews · doi:10.1039/c2cs35086f · Cited by 768
Porous Metal Oxides as Gas Sensors
Tiemann, M. (2007) · Chemistry – A European Journal · doi:10.1002/chem.200700927 · Cited by 675
Metadata
- Authors
- Smarsly, B., Grosso, D., Brezesinski, T., Pinna, N., Boissière, C., Antonietti, M., & Sanchez, C.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-07-01
- Volume
- 16
- Issue
- 15
- Pages
- 2948-2952
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2005988014
- Cited by
- 313
- References
- 0
- FWCI
- 15.00
- Type
- journal article
- Language
- en
- Open access
- closed
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- Smarsly, B., Grosso, D., Brezesinski, T., Pinna, N., Boissière, C., Antonietti, M., & Sanchez, C. (2004). Highly Crystalline Cubic Mesoporous TiO2 with 10-nm Pore Diameter Made with a New Block Copolymer Template. Chemistry of Materials. https://doi.org/10.1021/cm0495966
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