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Controlled Synthesis of Ordered Mesoporous C−TiO2 Nanocomposites with Crystalline Titania Frameworks from Organic−Inorganic−Amphiphilic Coassembly
Abstract
Highly ordered mesoporous carbon−titania nanocomposites with nanocrystal-glass frameworks have been synthesized via the organic−inorganic−amphiphilic coassembly followed by the in situ crystallization technology. A soluble resol polymer was used as a carbon precursor, prehydrolyzed TiCl 4 as an inorganic precursor, and triblock copolymer F127 as a template. The carbon−titania nanocomposites with controllable texture properties and composition can be obtained in a wide range from 20 to 80 wt% TiO 2 by adjusting the initial mass ratios. The C−TiO 2 nanocomposites with “bricked-mortar”frameworks exhibit highly ordered 2D hexagonal mesostructure and high thermal stability up to 700 °C. The nanocomposites have high surface area (465 m 2 g −1 ) and large pore size (∼4.1 nm). Additionally, the nanocomposites show good performance in degradation of Rhodamine B due to the photocatalytic activity of the titania nanocrystals and the strong adsorptive capacity of the glasslike carbon.
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Cites
Generalized syntheses of large-pore mesoporous metal oxides with semicrystalline frameworks
Yang, P., Zhao, D., Margolese, D. I., Chmelka, B. F., & Stucky, G. D. (1998) · Nature · doi:10.1038/24132 · Cited by 2,493
Self-citation
Cited by
Hierarchically porous materials: synthesis strategies and structure design
Yang, X.-Y., Chen, L.-H., Li, Y., Rooke, J. C., Sanchez, C., & Su, B.-L. (2017) · Chemical Society Reviews · doi:10.1039/c6cs00829a · Cited by 1,439
Ordered mesoporous metal oxides: synthesis and applications
Ren, Y., Ma, Z., & Bruce, P. G. (2012) · Chemical Society Reviews · doi:10.1039/c2cs35086f · Cited by 768
Self-citationSynthesis of non-siliceous mesoporous oxides
Gu, D., & Schüth, F. (2014) · Chem. Soc. Rev. · doi:10.1039/c3cs60155b · Cited by 584
Orilall, M. C., & Wiesner, U. (2011) · Chem. Soc. Rev. · doi:10.1039/c0cs00034e · Cited by 520
Mesoporous titania photocatalysts: preparation, characterization and reaction mechanisms
Ismail, A. A., & Bahnemann, D. W. (2011) · Journal of Materials Chemistry · doi:10.1039/c1jm10407a · Cited by 454
Metadata
- Authors
- Liu, R., Ren, Y., Shi, Y., Zhang, F., Zhang, L., Tu, B., & Zhao, D.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-09-26
- Volume
- 20
- Issue
- 3
- Pages
- 1140-1146
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2080382848
- Cited by
- 196
- References
- 1
- FWCI
- 7.50
- Type
- journal article
- Language
- en
- Open access
- closed
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- Liu, R., Ren, Y., Shi, Y., Zhang, F., Zhang, L., Tu, B., & Zhao, D. (2008). Controlled Synthesis of Ordered Mesoporous C−TiO2 Nanocomposites with Crystalline Titania Frameworks from Organic−Inorganic−Amphiphilic Coassembly. Chemistry of Materials. https://doi.org/10.1021/cm071470w
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