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Deoxygenation of Graphene Oxide: Reduction or Cleaning?
Open accessAbstract
High Resolution Image Download MS PowerPoint Slide We show that the two-component model of graphene oxide (GO), that is, composed of highly oxidized carbonaceous debris complexed to oxygen functionalized graphene sheets, is a generic feature of the synthesis of GO, independent of oxidant or protocol used. The debris present, roughly one-third by mass, can be removed by a base wash. A number of techniques, including solid state NMR, demonstrate that the properties of the base-washed material are independent of the base used and that it contains similar functional groups to those present in the debris but at a lower concentration. Removal of the oxidation debris cleans the GO, revealing its true monolayer nature and in the process increases the C/O ratio (i.e., a deoxygenation). By contrast, treating GO with hydrazine both removes the debris and reduces (both deoxygenations) the graphene sheets.
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The chemistry of graphene oxide
Dreyer, D. R., Park, S., Bielawski, C. W., & Ruoff, R. S. (2010) · Chem. Soc. Rev. · doi:10.1039/b917103g · Cited by 11,653
Cited by
Chabot, V., Higgins, D., Yu, A., Xiao, X., Chen, Z., & Zhang, J. (2014) · Energy & Environmental Science · doi:10.1039/c3ee43385d · Cited by 1,119
Metadata
- Authors
- Thomas, H. R., Day, S. P., Woodruff, W. E., Vallés, C., Young, R. J., Kinloch, I. A., Morley, G. W., Hanna, J. V., Wilson, N. R., & Rourke, J. P.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-09-05
- Volume
- 25
- Issue
- 18
- Pages
- 3580-3588
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W1969340573
- Cited by
- 221
- References
- 1
- FWCI
- 10.51
- Type
- journal article
- Language
- en
- Open access
- hybrid
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- Thomas, H. R., Day, S. P., Woodruff, W. E., Vallés, C., Young, R. J., Kinloch, I. A., Morley, G. W., Hanna, J. V., Wilson, N. R., & Rourke, J. P. (2013). Deoxygenation of Graphene Oxide: Reduction or Cleaning? Chemistry of Materials. https://doi.org/10.1021/cm401922e
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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