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Formation of Ni3C Nanocrystals by Thermolysis of Nickel Acetylacetonate in Oleylamine: Characterization Using Hard X-ray Photoelectron Spectroscopy
Abstract
Nickel acetylacetonate was thermally decomposed in oleylamine under inert atmosphere. Nanocrystals of two cubic phases and a hexagonal phase appeared. The phases were identified using X-ray diffraction, laboratory X-ray photoelectron spectroscopy (XPS), and hard-X-ray photoelectron spectroscopy (HX-PES). The hexagonal phase was a nickel carbide, Ni 3 C, which had been often identified as a hexagonal close-packed metallic nickel. One cubic phase was a face-centered metallic nickel, and the other cubic phase was proposed as a novel cubic nickel carbide, which was characterized as an intermediate product of the carbidization of metallic face-centered cubic Ni to the hexagonal nickel carbide.
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Cited by
Qiu, H. ‐., Ito, Y., Cong, W., Tan, Y., Liu, P., Hirata, A., Fujita, T., Tang, Z., & Chen, M. (2015) · Angewandte Chemie International Edition · doi:10.1002/anie.201507381 · Cited by 756
Specific Solvent Produces Specific Phase Ni Nanoparticles: A Pulsed Laser Ablation in Solvents
Jung, H. J., & Choi, M. Y. (2014) · The Journal of Physical Chemistry C · doi:10.1021/jp503009a · Cited by 93
Qiu, H. ‐., Ito, Y., Cong, W., Tan, Y., Liu, P., Hirata, A., Fujita, T., Tang, Z., & Chen, M. (2015) · Angewandte Chemie · doi:10.1002/ange.201507381 · Cited by 87
Su, Y., Li, Z., Zhou, H., Kang, S., Zhang, Y., Yu, C., & Wang, G. (2020) · Chemical Engineering Journal · doi:10.1016/j.cej.2020.126205 · Cited by 78
Metadata
- Authors
- Goto, Y., Taniguchi, K., Omata, T., Otsuka-Yao-Matsuo, S., Ohashi, N., Ueda, S., Yoshikawa, H., Yamashita, Y., Oohashi, H., & Kobayashi, K.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2008-06-01
- Volume
- 20
- Issue
- 12
- Pages
- 4156-4160
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2005044921
- Cited by
- 190
- References
- 0
- FWCI
- 1.87
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: Formation of Ni3C Nanocrystals by Thermolysis of Nickel Acetylacetonate in Oleylamine: Characterization Using Hard X-ray Photoelectron Spectroscopy. https://app.cochat.ai/papers/10.1021/cm703644x
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- Goto, Y., Taniguchi, K., Omata, T., Otsuka-Yao-Matsuo, S., Ohashi, N., Ueda, S., Yoshikawa, H., Yamashita, Y., Oohashi, H., & Kobayashi, K. (2008). Formation of Ni3C Nanocrystals by Thermolysis of Nickel Acetylacetonate in Oleylamine: Characterization Using Hard X-ray Photoelectron Spectroscopy. Chemistry of Materials. https://doi.org/10.1021/cm703644x
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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