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Synthesis of CdS and CdSe Nanocrystallites Using a Novel Single-Molecule Precursors Approach
Open accessAbstract
The synthesis of CdS and CdSe nanocrystallites using the thermolysis of several dithio- or diselenocarbamato complexes of cadmium in trioctylphosphine oxide (TOPO) is reported. The nanodispersed materials obtained show quantum size effects in their optical spectra and exhibit near band-edge luminescence. The influence of experimental parameters on the properties of the nanocrystallites is discussed. HRTEM images of these materials show well-defined, crystalline nanosized particles. Standard size fractionation procedures can be performed in order to narrow the size dispersion of the samples. The TOPO-capped CdS and CdSe nanocrystallites and simple organic bridging ligands, such as 2,2‘-bipyrimidine, are used as the starting materials for the preparation of novel nanocomposites. The optical properties shown by these new nanocomposites are compared with those of the starting nanodispersed materials.
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Cited by
Moriarty, P. (2001) · Reports on Progress in Physics · doi:10.1088/0034-4885/64/3/201 · Cited by 785
Castro, S. L., Bailey, S. G., Raffaelle, R. P., Banger, K. K., & Hepp, A. F. (2004) · The Journal of Physical Chemistry B · doi:10.1021/jp049107p · Cited by 434
The Heat-Up Synthesis of Colloidal Nanocrystals
van Embden, J., Chesman, A. S. R., & Jasieniak, J. J. (2015) · Chemistry of Materials · doi:10.1021/cm5028964 · Cited by 414
Shape Control of II–VI Semiconductor Nanomaterials
Kumar, S., & Nann, T. (2006) · Small · doi:10.1002/smll.200500357 · Cited by 386
SYNTHESIS ROUTES FOR LARGE VOLUMES OF NANOPARTICLES
Masala, O., & Seshadri, R. (2004) · Annual Review of Materials Research · doi:10.1146/annurev.matsci.34.052803.090949 · Cited by 355
Metadata
- Authors
- Trindade, T., O'Brien, P., & Zhang, X.-M.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 1997-02-01
- Volume
- 9
- Issue
- 2
- Pages
- 523-530
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2050108129
- Cited by
- 282
- References
- 0
- FWCI
- 7.84
- Type
- journal article
- Language
- en
- Open access
- green
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- Trindade, T., O'Brien, P., & Zhang, X.-M. (1997). Synthesis of CdS and CdSe Nanocrystallites Using a Novel Single-Molecule Precursors Approach. Chemistry of Materials. https://doi.org/10.1021/cm960363r
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