The DOI matches its Crossref record; 2 of the 2 references it cites were found in a registry or an index.
A New Synthesis of Mesoporous MSU-X Silica Controlled by a Two-Step Pathway
Abstract
In the field of micelle templated structures (MTS), the MSU-X family of mesoporous silica is obtained by using nonionic poly(ethylene oxide)-based surfactants. We show that the microstructure of these materials is highly dependent on the initial pH conditions and that a first assembly step, using a mild acidity, which allowed us to obtain a stable solution containing micellar hybrid objects made of both surfactant micelles and small silica oligomers, can be determined in the 2−4 pH range. The second step of the synthesis consists of the condensation of the silica particles and can be performed in two different ways. Either the pH of the stable solution is increased to neutral values or small amounts of fluoride are added. With the second method both the nanostructure and the particle morphology are better controlled. This novel two-step synthesis leads in addition to hexagonal pore framework when assembly molecules such as Tween 60 or block copolymer Pluronic P123 are used as assembly agents.
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Citations
Cites
Adsorption of Gases in Multimolecular Layers
Brunauer, S., Emmett, P. H., & Teller, E. (1938) · Journal of the American Chemical Society · doi:10.1021/ja01269a023 · Cited by 28,156
On a theory of the van der waals adsorption of gases
Brunauer, S., Deming, L. S., Deming, W. E., & Teller, E. (1940) · Journal of the American Chemical Society · doi:10.1021/ja01864a025 · Cited by 4,829
Cited by
Direct Synthesis of Al−SBA-15 Mesoporous Materials via Hydrolysis-Controlled Approach
Li, Y., Zhang, W., Zhang, L., Yang, Q., Wei, Z., Feng, Z., & Li, C. (2004) · The Journal of Physical Chemistry B · doi:10.1021/jp049824j · Cited by 260
Metadata
- Authors
- Boissière, C., Larbot, A., van der Lee, A., Kooyman, P. J., & Prouzet, E.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2000-09-15
- Volume
- 12
- Issue
- 10
- Pages
- 2902-2913
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W1995578811
- Cited by
- 206
- References
- 2
- FWCI
- 7.65
- Type
- journal article
- Language
- en
- Open access
- closed
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