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Electron Tomography for Heterogeneous Catalysts and Related Nanostructured Materials
Abstract
A comprehensive overview to the rapidly emerging field of electron tomography (ET) for the study of heterogeneous catalysts and related nanostructured materials is presented. The study includes a detailed analysis of materials classes of zeolites, ordered mesoporous materials, disordered oxide supported catalysts, carbon materials, and miscellaneous materials such as ceramics, polymers, and nanocomposites. ET includes collecting a series of 2D images by tilting the specimen in the electron beam and recording an image at each tilt step. Common academic and commercial software packages are utilized for the alignment and reconstruction of ET data of these material samples. A detailed assessment of the validity for BF TEM ET shows that for weakly scattering materials where mass thickness is the dominant contrast mechanism, electron microscope images are essentially projections on which a tomographic reconstruction can be based.
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Cites
Characterization of the porous structure of sba-15
Kruk, M., Jaroniec, M., Ko, C. H., & Ryoo, R. (2000) · Chemistry of Materials · doi:10.1021/cm000164e · Cited by 1,409
Cited by
Ray, P. C. (2010) · Chemical Reviews · doi:10.1021/cr900335q · Cited by 773
Three-dimensional analysis of Nafion layers in fuel cell electrodes
Lopez-Haro, M., Guétaz, L., Printemps, T., Morin, A., Escribano, S., Jouneau, P.-H., Bayle-Guillemaud, P., Chandezon, F., & Gebel, G. (2014) · Nature Communications · doi:10.1038/ncomms6229 · Cited by 402
Mesopore quality determines the lifetime of hierarchically structured zeolite catalysts
Milina, M., Mitchell, S., Crivelli, P., Cooke, D., & Pérez-Ramírez, J. (2014) · Nature Communications · doi:10.1038/ncomms4922 · Cited by 351
Visualization of hierarchically structured zeolite bodies from macro to nano length scales
Mitchell, S., Michels, N.-L., Kunze, K., & Pérez-Ramírez, J. (2012) · Nature Chemistry · doi:10.1038/nchem.1403 · Cited by 270
Metadata
- Authors
- Friedrich, H., de Jongh, P. E., Verkleij, A. J., & de Jong, K. P.
- Venue
- Chemical Reviews
- Publisher
- American Chemical Society (ACS)
- Published
- 2009-03-20
- Volume
- 109
- Issue
- 5
- Pages
- 1613-1629
- ISSN
- 0009-2665 (ISSN-L)
- 1520-6890
- OpenAlex
- W2168518481
- Cited by
- 256
- References
- 1
- FWCI
- 2.26
- Type
- journal article
- Language
- en
- Open access
- closed
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- Friedrich, H., de Jongh, P. E., Verkleij, A. J., & de Jong, K. P. (2009). Electron Tomography for Heterogeneous Catalysts and Related Nanostructured Materials. Chemical Reviews. https://doi.org/10.1021/cr800434t
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