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Hierarchical FeWO4 Microcrystals: Solvothermal Synthesis and Their Photocatalytic and Magnetic Properties
Abstract
Highly hierarchical platelike FeWO(4) microcrystals have been synthesized by a simple solvothermal route using FeCl(3) x 6 H(2)O and Na(2)WO(4) x 2 H(2)O as precursors, where ethylene glycol (EG) plays an important role as a capping agent in directing growth and self-assembly of such unique structures. In addition, a certain amount of CH(3)COONa (NaAc) was necessary for the formation of such unique FeWO(4) microstructures. The photocatalytic property of as-synthesized hierarchical FeWO(4) microcrystals has been first studied, which shows excellent photocatalytic activity for the degradation of rhodamine B (RhB) under UV and visible light irradiation (modeling sunlight). Moreover, magnetic measurement indicates that hexangular FeWO(4) platelike microcrystals show a small ferromagnetic ordering at low temperature because of spin-canting of antiferromagnetic materials and surface spins of FeWO(4) nanoparticles.
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Cites
Anisotropic Superexchange Interaction and Weak Ferromagnetism
Moriya, T. (1960) · Physical Review · doi:10.1103/physrev.120.91 · Cited by 7,234
Cited by
3D hierarchical flower-like TiO2 nanostructure: morphology control and its photocatalytic property
Tian, G., Chen, Y., Zhou, W., Pan, K., Tian, C., Huang, X.-R., & Fu, H. (2011) · CrystEngComm · doi:10.1039/c0ce00851f · Cited by 259
Wu, X., Bao, C., Niu, Q., & Lu, W. (2019) · Nanotechnology · doi:10.1088/1361-6528/aafe53 · Cited by 28
Metadata
- Authors
- Zhou, Y.-X., Yao, H.-B., Zhang, Q., Gong, J.-Y., Liu, S.-J., & Yu, S.-H.
- Venue
- Inorganic Chemistry
- Publisher
- American Chemical Society (ACS)
- Published
- 2009-01-06
- Volume
- 48
- Issue
- 3
- Pages
- 1082-1090
- ISSN
- 0020-1669 (ISSN-L)
- 1520-510X
- OpenAlex
- W2083510097
- Cited by
- 220
- References
- 1
- FWCI
- 10.44
- Type
- journal article
- Language
- en
- Open access
- closed
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- Zhou, Y.-X., Yao, H.-B., Zhang, Q., Gong, J.-Y., Liu, S.-J., & Yu, S.-H. (2009). Hierarchical FeWO4 Microcrystals: Solvothermal Synthesis and Their Photocatalytic and Magnetic Properties. Inorganic Chemistry. https://doi.org/10.1021/ic801806r
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