The DOI matches its Crossref record; 2 of the 2 references it cites were found in a registry or an index.
Selective Conversion of D-Fructose to 5-Hydroxymethylfurfural by Ion-Exchange Resin in Acetone/Dimethyl sulfoxide Solvent Mixtures
Open accessAbstract
Catalytic dehydration of D -fructose to 5-Hydroxymethylfurfural (5-HMF) in acetone/dimethyl sulfoxide solvent mixtures was studied in the presence of a strong acidic cation-exchange resin catalyst (DOWEX 50WX8−100) by microwave heating. The addition of acetone to the dimethyl sulfoxide (DMSO) solvent promoted the formation of 5-HMF from D -fructose. For a D -fructose conversion of 97.9%, the 5-HMF selectivity was 91.7% for a 20-min reaction time in 70:30 (w/w) acetone/DMSO solvent mixtures. Concentrations as high as 10 wt % D -fructose were studied, for which it was found that 5-HMF yields of 82.1% for a reaction time of 10 min could be obtained. The stability of the ion-exchange resin used as the catalyst was confirmed. Compared to pure DMSO solvent, the combination of low-boiling-point acetone with DMSO used as the reaction medium not only gives highly selective 5-HMF formation, but also improves the separation efficiency and reduces environmental risk.
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Citations
Cites
Metal Chlorides in Ionic Liquid Solvents Convert Sugars to 5-Hydroxymethylfurfural
Zhao, H., Holladay, J. E., Brown, H., & Zhang, Z. C. (2007) · Science · doi:10.1126/science.1141199 · Cited by 1,997
Acid-Catalyzed Production of 5-Hydroxymethyl Furfural from d-Fructose in Subcritical Water
Salak Asghari, F., & Yoshida, H. (2006) · Industrial & Engineering Chemistry Research · doi:10.1021/ie051088y · Cited by 500
Cited by
Bozell, J. J., & Petersen, G. R. (2010) · Green Chemistry · doi:10.1039/b922014c · Cited by 4,566
Hydroxymethylfurfural, A Versatile Platform Chemical Made from Renewable Resources
van Putten, R.-J., van der Waal, J. C., de Jong, E., Rasrendra, C. B., Heeres, H. J., & de Vries, J. G. (2013) · Chemical Reviews · doi:10.1021/cr300182k · Cited by 2,886
Biomass into chemicals: Conversion of sugars to furan derivatives by catalytic processes
Tong, X., Ma, Y., & Li, Y. (2010) · Applied Catalysis A: General · doi:10.1016/j.apcata.2010.06.049 · Cited by 847
Zakrzewska, M. E., Bogel-Łukasik, E., & Bogel-Łukasik, R. (2011) · Chemical Reviews · doi:10.1021/cr100171a · Cited by 800
Choudhary, V., Mushrif, S. H., Ho, C., Anderko, A., Nikolakis, V., Marinkovic, N. S., Frenkel, A. I., Sandler, S. I., & Vlachos, D. G. (2013) · Journal of the American Chemical Society · doi:10.1021/ja3122763 · Cited by 685
Metadata
- Authors
- Qi, X., Watanabe, M., Aida, T. M., & Smith, R. L.
- Venue
- Industrial & Engineering Chemistry Research
- Publisher
- American Chemical Society (ACS)
- Published
- 2008-11-01
- Volume
- 47
- Issue
- 23
- Pages
- 9234-9239
- ISSN
- 0888-5885 (ISSN-L)
- 1520-5045
- OpenAlex
- W2027167320
- Cited by
- 180
- References
- 2
- FWCI
- 8.10
- Type
- journal article
- Language
- en
- Open access
- bronze
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- Qi, X., Watanabe, M., Aida, T. M., & Smith, R. L. (2008). Selective Conversion of D-Fructose to 5-Hydroxymethylfurfural by Ion-Exchange Resin in Acetone/Dimethyl sulfoxide Solvent Mixtures. Industrial & Engineering Chemistry Research. https://doi.org/10.1021/ie801016s
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