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Nonionic Block Copolymer Synthesis of Large-Pore Cubic Mesoporous Single Crystals by Use of Inorganic Salts
Abstract
Large-pore cubic (Im3m) mesoporous silica single crystals have been synthesized by using commercial nonionic block copolymers as templates and inorganic salts as additives. These single crystals possess exclusively uniform rhombdodecahedron shapes ( approximately 1 mum) with approximately 100% yield. The mesopore lattice array in each crystal face is solved by TEM, further confirming that these crystals are perfect single crystals.
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Citations
Cited by
On the controllable soft-templating approach to mesoporous silicates
Wan, Y., & Zhao (2007) · Chemical Reviews · doi:10.1021/cr068020s · Cited by 2,371
Liu, J., Qiao, S. Z., Liu, H., Chen, J., Orpe, A., Zhao, D., & Lu, G. Q. (. (2011) · Angewandte Chemie International Edition · doi:10.1002/anie.201102011 · Cited by 871
Self-citationA novel anionic surfactant templating route for synthesizing mesoporous silica with unique structure
Che, S., Garcia-Bennett, A. E., Yokoi, T., Sakamoto, K., Kunieda, H., Terasaki, O., & Tatsumi, T. (2003) · Nature Materials · doi:10.1038/nmat1022 · Cited by 564
Block copolymer-templated mesoporous oxides
Soler-Illia, G. J. D. A. A., Crepaldi, E. L., Grosso, D., & Sanchez, C. (2003) · Current Opinion in Colloid & Interface Science · doi:10.1016/s1359-0294(03)00002-5 · Cited by 501
Design and fabrication of mesoporous heterogeneous basic catalysts
Sun, L.-B., Liu, X.-Q., & Zhou, H.-C. (2015) · Chemical Society Reviews · doi:10.1039/c5cs00090d · Cited by 386
Metadata
- Authors
- Yu, C., Tian, B., Fan, J., Stucky, G. D., & Zhao, D.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2002-04-02
- Volume
- 124
- Issue
- 17
- Pages
- 4556-4557
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W1970943379
- Cited by
- 312
- References
- 0
- FWCI
- 16.14
- Type
- journal article
- Language
- en
- Open access
- closed
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- Yu, C., Tian, B., Fan, J., Stucky, G. D., & Zhao, D. (2002). Nonionic Block Copolymer Synthesis of Large-Pore Cubic Mesoporous Single Crystals by Use of Inorganic Salts. Journal of the American Chemical Society. https://doi.org/10.1021/ja025548f
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
