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Benzyl Alcohol and Transition Metal Chlorides as a Versatile Reaction System for the Nonaqueous and Low-Temperature Synthesis of Crystalline Nano-Objects with Controlled Dimensionality
Abstract
The reaction of transition metal chlorides with benzyl alcohol leads at low temperatures to oxidic nanostructures with low-dimensional particle shapes such as nearly spherical titania anatase nanoparticles, vanadium oxide nanorods, and tungsten oxide nanoplatelets. The process is simple, allows a scale-up in gram quantities, and leads to highly crystalline materials. Ethanol solutions containing tungsten oxide nanoparticles exhibit blue luminescence upon UV irradiation at room temperature.
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Citations
Cited by
Nonaqueous sol–gel routes to metal oxide nanoparticles
Niederberger, M. (2007) · Accounts of Chemical Research · doi:10.1021/ar600035e · Cited by 761
Self-citationPolleux, J., Gurlo, A., Barsan, N., Weimar, U., Antonietti, M., & Niederberger, M. (2006) · Angewandte Chemie International Edition · doi:10.1002/anie.200502823 · Cited by 369
Self-citationMagnetite Nanocrystals: Nonaqueous Synthesis, Characterization, and Solubility
Pinna, N., Grancharov, S., Beato, P., Bonville, P., Antonietti, M., & Niederberger, M. (2005) · Chemistry of Materials · doi:10.1021/cm050060+ · Cited by 355
Self-citationNiederberger, M., Garnweitner, G., Pinna, N., & Antonietti, M. (2004) · Journal of the American Chemical Society · doi:10.1021/ja0494959 · Cited by 284
Self-citationJoo, J., Kwon, S. G., Yu, J. H., & Hyeon, T. (2005) · Advanced Materials · doi:10.1002/adma.200402109 · Cited by 277
Metadata
- Authors
- Niederberger, M., Bartl, M. H., & Stucky, G. D.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2002-10-30
- Volume
- 124
- Issue
- 46
- Pages
- 13642-13643
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2091074451
- Cited by
- 360
- References
- 0
- FWCI
- 8.89
- Type
- journal article
- Language
- en
- Open access
- closed
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- Niederberger, M., Bartl, M. H., & Stucky, G. D. (2002). Benzyl Alcohol and Transition Metal Chlorides as a Versatile Reaction System for the Nonaqueous and Low-Temperature Synthesis of Crystalline Nano-Objects with Controlled Dimensionality. Journal of the American Chemical Society. https://doi.org/10.1021/ja027115i
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
