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One-Step Nanocasting Synthesis of Highly Ordered Single Crystalline Indium Oxide Nanowire Arrays from Mesostructured Frameworks
Abstract
A one-step nanocasting route has been demonstrated to prepare highly ordered single-crystal indium oxide nanowire (IONW) arrays with mesostructured frameworks. Unlike the reported multistep nanocasting process (synthesis of mesoporous materials, and then incorporation of precursors and formation of inorganic frameworks), a highly ordered mesostructured surfactant-silica monolith with low external surface serves as both the template and the reducing agent and makes the formation of single-crystal IONWs in its channels easily in one step by using normal In(NO(3))(3) as an inorganic precursor. After silica is removed, highly ordered uniform single-crystal IONW arrays with hexagonal (p6mm) or cubic (Ia3d) mesostructures are derived. These new materials are studied by XRD, SEM, TEM, N(2) adsoption, and UV spectrum. Furthermore, this one-step nanocasting synthesis route is a generalized method and can be used to synthesized a highly ordered mesoporous silica monolith with metal oxide nanocrystals in its channels. To the best of our knowledge, this is the first report of a single crystalline mesostructured In(2)O(3) framework.
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Citations
Cited by
Ordered mesoporous materials in catalysis
Taguchi, A., & Schüth, F. (2005) · Microporous and Mesoporous Materials · doi:10.1016/j.micromeso.2004.06.030 · Cited by 2,119
Kim, T.-W., Kleitz, F., Paul, B., & Ryoo, R. (2005) · Journal of the American Chemical Society · doi:10.1021/ja042601m · Cited by 733
On the Synergetic Catalytic Effect in Heterogeneous Nanocomposite Catalysts
Shi, J. (2013) · Chemical Reviews · doi:10.1021/cr3002752 · Cited by 652
Metadata
- Authors
- Yang, H., Shi, Q., Tian, B., Lu, Q., Gao, F., Xie, S., Fan, J., Yu, C., Tu, B., & Zhao, D.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2003-03-29
- Volume
- 125
- Issue
- 16
- Pages
- 4724-4725
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2018864861
- Cited by
- 205
- References
- 0
- FWCI
- 12.29
- Type
- journal article
- Language
- en
- Open access
- closed
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