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Diluting Abundant Spins by Isotope Edited Radio Frequency Field Assisted Diffusion
Abstract
A new solid-state NMR method is described for obtaining long-range distance constraints in nanocrystalline samples of 13C-, 15N-, and 2H-enriched protein. The method selects only those 13C or 15N nuclei close to 1Hs for dipolar recoupling. When used with extensive deuteration, the bath of abundant 13C spins is made to appear dilute. Contacts over 4.5 A are readily observed in human ubiquitin.
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Cited by
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Petkova, A. T., Yau, W.-M., & Tycko, R. (2006) · Biochemistry · doi:10.1021/bi051952q · Cited by 1,044
Luca, S., Yau, W.-M., Leapman, R., & Tycko, R. (2007) · Biochemistry · doi:10.1021/bi701427q · Cited by 578
Hou, G., Yan, S., Trébosc, J., Amoureux, J.-P., & Polenova, T. (2013) · Journal of Magnetic Resonance · doi:10.1016/j.jmr.2013.04.009 · Cited by 193
Lesage, A., Emsley, L., Penin, F., & Böckmann, A. (2006) · Journal of the American Chemical Society · doi:10.1021/ja060866q · Cited by 77
Metadata
- Authors
- Morcombe, C. R., Gaponenko, V., Byrd, R. A., & Zilm, K. W.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-05-20
- Volume
- 126
- Issue
- 23
- Pages
- 7196-7197
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2034121963
- Cited by
- 223
- References
- 0
- FWCI
- 4.00
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: Diluting Abundant Spins by Isotope Edited Radio Frequency Field Assisted Diffusion. https://app.cochat.ai/papers/10.1021/ja047919t
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- Morcombe, C. R., Gaponenko, V., Byrd, R. A., & Zilm, K. W. (2004). Diluting Abundant Spins by Isotope Edited Radio Frequency Field Assisted Diffusion. Journal of the American Chemical Society. https://doi.org/10.1021/ja047919t
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