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On the Mechanism of Lead Chalcogenide Nanocrystal Formation
Abstract
On the basis of evidence from 31P NMR spectroscopy, and using PbSe as a model, we propose two simultaneous mechanisms through which "monomers" are formed in preparations of lead chalcogenide nanocrystals (NCs). In one mechanism, selenium is delivered as a Se2- species, whereas in the other, Se0 reacts with metal already reduced by the organophosphine. This latter mechanism helps explain the sensitivity of NC preparations to the purity of organophosphines and allows the rational modification of batch NC reactions to increase yield.
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Peng, X., Wickham, J., & Alivisatos, A. P. (1998) · Journal of the American Chemical Society · doi:10.1021/ja9805425 · Cited by 1,895
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Liu, F., Zhang, Y., Ding, C., Kobayashi, S., Izuishi, T., Nakazawa, N., Toyoda, T., Ohta, T., Hayase, S., Minemoto, T., et al. (2017) · ACS Nano · doi:10.1021/acsnano.7b05442 · Cited by 960
Nonaqueous sol–gel routes to metal oxide nanoparticles
Niederberger, M. (2007) · Accounts of Chemical Research · doi:10.1021/ar600035e · Cited by 761
Synthesis and properties of colloidal heteronanocrystals
Donegá, C. D. M. (2011) · Chem. Soc. Rev. · doi:10.1039/c0cs00055h · Cited by 719
Law, M., Luther, J. M., Song, Q., Hughes, B. K., Perkins, C. L., & Nozik, A. J. (2008) · Journal of the American Chemical Society · doi:10.1021/ja800040c · Cited by 431
Metadata
- Authors
- Steckel, J. S., Yen, B. K. H., Oertel, D. C., & Bawendi, M. G.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2006-09-16
- Volume
- 128
- Issue
- 40
- Pages
- 13032-13033
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2073102782
- Cited by
- 302
- References
- 1
- FWCI
- 8.46
- Type
- journal article
- Language
- en
- Open access
- closed
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