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A Versatile Kinetics-Controlled Coating Method To Construct Uniform Porous TiO2 Shells for Multifunctional Core–Shell Structures
Abstract
The development of a simple and reproducible route to prepare uniform core@TiO(2) structures is urgent for realizing multifunctional responses and harnessing multiple interfaces for new or enhanced functionalities. Here, we report a versatile kinetics-controlled coating method to construct uniform porous TiO(2) shells for multifunctional core-shell structures. By simply controlling the kinetics of hydrolysis and condensation of tetrabutyl titanate (TBOT) in ethanol/ammonia mixtures, uniform porous TiO(2) shell core-shell structures can be prepared with variable diameter, geometry, and composition as a core (e.g., α-Fe(2)O(3) ellipsoids, Fe(3)O(4) spheres, SiO(2) spheres, graphene oxide nanosheets, and carbon nanospheres). This method is very simple and reproducible, yet important, which allows an easy control over the thickness of TiO(2) shells from 0 to ~25, ~45, and ~70 nm. Moreover, the TiO(2) shells possess large mesoporosities and a uniform pore size of ~2.5 nm, and can be easily crystallized into anatase phase without changing the uniform core-shell structures.
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Cites
Theory, Production and Mechanism of Formation of Monodispersed Hydrosols
LaMer, V. K., & Dinegar, R. H. (1950) · Journal of the American Chemical Society · doi:10.1021/ja01167a001 · Cited by 3,894
Cited by
Liu, X., Xing, Z., Zhang, Y., Li, Z., Wu, X., Tan, S., Yu, X., Zhu, Q., & Zhou, W. (2017) · Applied Catalysis B: Environmental · doi:10.1016/j.apcatb.2016.08.031 · Cited by 367
Qi, Z., Xiao, C., Liu, C., Goh, T. W., Zhou, L., Maligal-Ganesh, R., Pei, Y., Li, X., Curtiss, L. A., & Huang, W. (2017) · Journal of the American Chemical Society · doi:10.1021/jacs.6b12780 · Cited by 331
Du, D., Shi, W., Wang, L., & Zhang, J. (2017) · Applied Catalysis B: Environmental · doi:10.1016/j.apcatb.2016.07.043 · Cited by 266
Metadata
- Authors
- Li, W., Yang, J., Wu, Z., Wang, J., Li, B., Feng, S., Deng, Y., Zhang, F., & Zhao, D.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2012-07-05
- Volume
- 134
- Issue
- 29
- Pages
- 11864-11867
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2333038000
- Cited by
- 446
- References
- 1
- FWCI
- 17.23
- Type
- journal article
- Language
- en
- Open access
- closed
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- Li, W., Yang, J., Wu, Z., Wang, J., Li, B., Feng, S., Deng, Y., Zhang, F., & Zhao, D. (2012). A Versatile Kinetics-Controlled Coating Method To Construct Uniform Porous TiO2 Shells for Multifunctional Core–Shell Structures. Journal of the American Chemical Society. https://doi.org/10.1021/ja3037146
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Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
